cabenegrin A-II

Base Information

Chemical Name:cabenegrin A-II
CAS No.:84297-60-9
Molecular Formula:C₂₁H₂₂O₆
Molecular Weight:370.402
Hs Code.:
UNII:6D0K52WN5Y
Nikkaji Number:J1.568.135G
Wikidata:Q27264528

Synonyms:cabenegrin A-II;Cabenegrin A II;(-)-Cabenegrin A II;Cabenegrin A-II [MI];UNII-6D0K52WN5Y;6D0K52WN5Y;84297-60-9;6H-(1,3)Dioxolo(5,6)benzofuro(3,2-C)(1)benzopyran-2-butanol, 6a,12a-dihydro-3-hydroxy-beta-methyl-, (6aR,12aR)-;SCHEMBL23043828;Q27264528;6H-(1,3)DIOXOLO(5,6)BENZOFURO(3,2-C)(1)BENZOPYRAN-2-BUTANOL, 6A,12A-DIHYDRO-3-HYDROXY-.BETA.-METHYL-, (6AR,12AR)-

Suppliers and Price of cabenegrin A-II

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cabenegrin A-II

Chemical Property:

Vapor Pressure:2.63E-12mmHg at 25°C
Boiling Point:535.7°Cat760mmHg
Flash Point:277.8°C
PSA：77.38000
Density:1.36g/cm³
LogP:3.29160
XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:370.14163842
Heavy Atom Count:27
Complexity:529

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CCC1=CC2=C(C=C1O)OCC3C2OC4=CC5=C(C=C34)OCO5)CO
Isomeric SMILES:CC(CCC1=CC2=C(C=C1O)OC[C@@H]3[C@H]2OC4=CC5=C(C=C34)OCO5)CO

Technology Process of cabenegrin A-II

There total 9 articles about cabenegrin A-II which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2150-47-2
methyl 2,4-dihydroxybenzoate

: 84297-60-9,84710-83-8
(+/-)-cabenegrin A-II

Guidance literature:: Multi-step reaction with 8 steps

1: K₂CO₃ / acetone / Heating

2: K₂CO₃, KI / acetone / Heating

3: N,N-diethylaniline / Heating

4: 30 percent / lithium chloropalladite / acetonitrile; H₂O

5: lithium aluminum hydride / tetrahydrofuran / -20 °C

6: 94 percent / manganese dioxide / CH₂Cl₂ / 7 h / Ambient temperature

7: 74 percent

8: H₂ / 10percent Pd-C

With manganese(IV) oxide; lithium aluminium tetrahydride; lithium tetrachloropalladate(II); hydrogen; potassium carbonate; N,N-diethylaniline; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
DOI:10.1016/S0040-4039(00)87727-8

Reference yield:

: 61080-20-4
2-(chloromercurio)-4,5-(methylenedioxy)phenol

: 84297-60-9,84710-83-8
(+/-)-cabenegrin A-II

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / lithium chloropalladite / acetonitrile; H₂O

2: lithium aluminum hydride / tetrahydrofuran / -20 °C

3: 94 percent / manganese dioxide / CH₂Cl₂ / 7 h / Ambient temperature

4: 74 percent

5: H₂ / 10percent Pd-C

With manganese(IV) oxide; lithium aluminium tetrahydride; lithium tetrachloropalladate(II); hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1016/S0040-4039(00)87727-8

Reference yield:

: 84666-41-1
methyl 2-hydroxy-4-propargyloxybenzoate

: 84297-60-9,84710-83-8
(+/-)-cabenegrin A-II

Guidance literature:: Multi-step reaction with 7 steps

1: K₂CO₃, KI / acetone / Heating

2: N,N-diethylaniline / Heating

3: 30 percent / lithium chloropalladite / acetonitrile; H₂O

4: lithium aluminum hydride / tetrahydrofuran / -20 °C

5: 94 percent / manganese dioxide / CH₂Cl₂ / 7 h / Ambient temperature

6: 74 percent

7: H₂ / 10percent Pd-C

With manganese(IV) oxide; lithium aluminium tetrahydride; lithium tetrachloropalladate(II); hydrogen; potassium carbonate; N,N-diethylaniline; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
DOI:10.1016/S0040-4039(00)87727-8