3-Cyclohexene-1-methanol, 2-[(2S,3S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-3-(methoxymethoxy)- 4-pentenyl]-3-methyl-6-(1-methylethyl)-, (1R,2R,6R)-

Base Information

Chemical Name:3-Cyclohexene-1-methanol, 2-[(2S,3S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-3-(methoxymethoxy)- 4-pentenyl]-3-methyl-6-(1-methylethyl)-, (1R,2R,6R)-
CAS No.:849122-90-3
Molecular Formula:C34H50O4Si
Molecular Weight:550.854
Hs Code.:

3-Cyclohexene-1-methanol,
2-[(2S,3S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-3-(methoxymethoxy)-
4-pentenyl]-3-methyl-6-(1-methylethyl)-, (1R,2R,6R)-

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Chemical Property of 3-Cyclohexene-1-methanol, 2-[(2S,3S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-3-(methoxymethoxy)- 4-pentenyl]-3-methyl-6-(1-methylethyl)-, (1R,2R,6R)-

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Technology Process of 3-Cyclohexene-1-methanol, 2-[(2S,3S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-3-(methoxymethoxy)- 4-pentenyl]-3-methyl-6-(1-methylethyl)-, (1R,2R,6R)-

There total 4 articles about 3-Cyclohexene-1-methanol, 2-[(2S,3S)-2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-3-(methoxymethoxy)- 4-pentenyl]-3-methyl-6-(1-methylethyl)-, (1R,2R,6R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849122-77-6
(2S,3S)-1-((1R,5R,6R)-6-Dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enyl)-3-methoxymethoxy-pent-4-en-2-ol

: 849122-90-3
{(1R,2R,6R)-2-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methoxymethoxy-pent-4-enyl]-6-isopropyl-3-methyl-cyclohex-3-enyl}-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / imidazole / CH₂Cl₂ / 16 h / 0 - 20 °C

2: 100 percent / AcOH / tetrahydrofuran; H₂O / 15 h / 20 °C

3: 71 percent / NaBH₄ / ethanol / 0.33 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2004.12.039

Reference yield:

: 849122-88-9
tert-Butyl-[(1S,2S)-1-((1R,5R,6R)-6-dimethoxymethyl-5-isopropyl-2-methyl-cyclohex-2-enylmethyl)-2-methoxymethoxy-but-3-enyloxy]-diphenyl-silane

: 849122-90-3
{(1R,2R,6R)-2-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methoxymethoxy-pent-4-enyl]-6-isopropyl-3-methyl-cyclohex-3-enyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / AcOH / tetrahydrofuran; H₂O / 15 h / 20 °C

2: 71 percent / NaBH₄ / ethanol / 0.33 h / 20 °C

With sodium tetrahydroborate; acetic acid; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.tet.2004.12.039

Reference yield:

: 62322-45-6
allyl methoxymethyl ether

: 849122-90-3
{(1R,2R,6R)-2-[(2S,3S)-2-(tert-Butyl-diphenyl-silanyloxy)-3-methoxymethoxy-pent-4-enyl]-6-isopropyl-3-methyl-cyclohex-3-enyl}-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / lIpc₂BOMe; sec-BuLi; BF₃*Et₂O / tetrahydrofuran / 16 h / -78 - -20 °C

2: 88 percent / imidazole / CH₂Cl₂ / 16 h / 0 - 20 °C

3: 100 percent / AcOH / tetrahydrofuran; H₂O / 15 h / 20 °C

4: 71 percent / NaBH₄ / ethanol / 0.33 h / 20 °C

With (-)-B-methoxydiisopinocamphenylborane; 1H-imidazole; sodium tetrahydroborate; boron trifluoride diethyl etherate; sec.-butyllithium; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2004.12.039