4-Pyridinecarboxylic acid, 2-ethyl-6-methyl-

Base Information

• Chemical Name: 4-Pyridinecarboxylic acid, 2-ethyl-6-methyl-
• CAS No.: 849226-46-6
• Molecular Formula: C9H11NO2
• Molecular Weight: 165.18900

Synonyms:

Chemical Property of 4-Pyridinecarboxylic acid, 2-ethyl-6-methyl-

Chemical Property:

• PSA: 50.19000
• LogP: 1.65060

Purity/Quality:

97% ^*data from raw suppliers

2-Ethyl-6-methylisonicotinicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Pyridinecarboxylic acid, 2-ethyl-6-methyl-

There total 1 articles about 4-Pyridinecarboxylic acid, 2-ethyl-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-ethyl-6-methyl-isonicotinic acid tert.-butyl ester (945463-90-1) → 2-ethyl-6-methyl-isonicotinic acid (849226-46-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

2-ethyl-6-methyl-isonicotinic acid (849226-46-6) + 4-benzyloxy-3,5-dimethyl-benzoic acid hydrazide (944327-04-2) → C25H27N3O3

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 3h;

Reference yield:

2-ethyl-6-methyl-isonicotinic acid (849226-46-6) + 4-benzyloxy-3,5-dimethyl-benzoic acid hydrazide (944327-04-2) → 4-[5-(4-benzyloxy-3,5-dimethyl-phenyl)-[1,3,4]oxadiazol-2-yl]-2-ethyl-6-methyl-pyridine (1011264-40-6)

Guidance literature:

2-ethyl-6-methyl-isonicotinic acid; 4-benzyloxy-3,5-dimethyl-benzoic acid hydrazide; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 3h;

With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 20 ℃; for 19h;

In dichloromethane; for 0.5h;

upstream raw materials:

2-ethyl-6-methyl-isonicotinic acid tert.-butyl ester

Downstream raw materials:

4-[5-(4-benzyloxy-3,5-dimethyl-phenyl)-[1,3,4]oxadiazol-2-yl]-2-ethyl-6-methyl-pyridine

C₂₆H₃₅N₃O₄

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