Methanesulfonic acid, trifluoro-, 3-fluoro-2-nitrophenyl ester

Base Information

Chemical Name:Methanesulfonic acid, trifluoro-, 3-fluoro-2-nitrophenyl ester
CAS No.:849353-43-1
Molecular Formula:C7H3F4NO5S
Molecular Weight:289.164
Hs Code.:2905190098

Synonyms:3-FLUORO-2-NITROPHENYL TRIFLUOROMETHANESULPHONATE;Methanesulfonic acid, trifluoro-, 3-fluoro-2-nitrophenyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanesulfonic acid, trifluoro-, 3-fluoro-2-nitrophenyl ester

Chemical Property:

PSA：97.57000
LogP:3.56630

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanesulfonic acid, trifluoro-, 3-fluoro-2-nitrophenyl ester

There total 2 articles about Methanesulfonic acid, trifluoro-, 3-fluoro-2-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 385-01-3
2-nitro-3-fluorophenol

: 849353-43-1
trifluoromethanesulfonic acid 3-fluoro-2-nitrophenyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.bmcl.2011.09.018

Reference yield:

: 372-20-3
3-fluorophenol

: 849353-43-1
trifluoromethanesulfonic acid 3-fluoro-2-nitrophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: nitronium tetrafluoborate / acetonitrile / 1 h / 0 °C

2: triethylamine / dichloromethane / 2 h / 0 °C

With nitronium tetrafluoborate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.09.018

Reference yield: 45.0%

: 849354-28-5
6-(5-fluoro-2-methylphenyl)-6-methyl-4-trifluoromethylhept-1-yn-4-ol

: 849353-43-1
trifluoromethanesulfonic acid 3-fluoro-2-nitrophenyl ester

: 849354-14-9
6-(5-fluoro-2-methylphenyl)-1-(3-fluoro-2-nitrophenyl)-6-methyl-4-trifluoromethylhept-1-yn-4-ol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; acetonitrile; at 20 ℃; for 18.5h;