Phenazine ethosulfate

Base Information

• Chemical Name: Phenazine ethosulfate
• CAS No.: 10510-77-7
• Deprecated CAS: 77898-71-6
• Molecular Formula: C14H13N2•C2H5O4S
• Molecular Weight: 334.396
• Hs Code.: 2933990090
• European Community (EC) Number: 234-044-9
• NSC Number: 402863
• UNII: 9A2K3Z3B9U
• DSSTox Substance ID: DTXSID4065101
• Mol file: 10510-77-7.mol

Synonyms:5-ethylphenazine;5-ethylphenazinium ethyl sulfate salt;N-ethyldibenzopyrazine ethyl sulfate;phenazine ethosulfate

Chemical Property of Phenazine ethosulfate

Chemical Property:

• Melting Point: 190 °C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 91.58000
• Density: g/cm³
• LogP: 3.25930
• Storage Temp.: Store at -20
• Solubility.: Aqueous Acid (Slightly), Methanol (Slightly), Water (Slightly)
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 334.09872823
• Heavy Atom Count: 23
• Complexity: 323

Purity/Quality:

99%, ^*data from raw suppliers

Phenazine ethosulfate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[N+]1=C2C=CC=CC2=NC3=CC=CC=C31.CCOS(=O)(=O)[O-]
• Uses: Phenazine Ethosulfate is an intermediate which is used to detect nitric oxide reducatase activity. Dyes and metabolites.

Technology Process of Phenazine ethosulfate

There total 1 articles about Phenazine ethosulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl sulfate (64-67-5) + Phenazin (92-82-0) → N-ethyldibenzopyrazine ethyl sulfate salt (10510-77-7)

Guidance literature:

DOI:10.1039/jr9370001704

Reference yield:

N-ethyldibenzopyrazine ethyl sulfate salt (10510-77-7) → C55H76N6O10P(1+)*C2H5O4S(1-)

Guidance literature:

Multi-step reaction with 3 steps

1: 44 percent / methanol / 1 h / Ambient temperature

2: 45 percent / tetrazole / acetonitrile / 0.75 h / 20 °C

3: 86 percent / TCA / methanol; CH₂Cl₂ / 3 h / 0 °C

With 1H-tetrazole; trichloroacetic acid; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/S0040-4020(97)00631-5

Reference yield:

N-ethyldibenzopyrazine ethyl sulfate salt (10510-77-7) → C74H90N6O11P(1+)*C2H5O4S(1-)

Guidance literature:

Multi-step reaction with 2 steps

1: 44 percent / methanol / 1 h / Ambient temperature

2: 45 percent / tetrazole / acetonitrile / 0.75 h / 20 °C

With 1H-tetrazole; In methanol; acetonitrile;

DOI:10.1016/S0040-4020(97)00631-5

upstream raw materials:

diethyl sulfate

Phenazin

Refernces

Synthesis and characterization of cis-4-decenoyl-CoA, 3-phenylpropionyl-CoA, and 2,6-dimethylheptanoyl-CoA

10.1016/j.ab.2010.02.026

The research focuses on the development of a method for synthesizing three medium-chain acyl-CoAs from unsaturated and less common fatty acids that are not commercially available. The key chemicals involved in this research include cis-4-decen-1-al, hydrocinnamic acid (3-phenylpropionic acid), anhydrous ethylchloroformate, ammonium formate, silver nitrate, thionyl chloride, 6-methyl-2-heptanol, p-toluenesulfonyl chloride, potassium phosphate, cytochrome c, potassium cyanide, phenazine ethosulfate, N-ethylmaleimide, rotenone, and CoASH (coenzyme A trilithium salt). These chemicals play crucial roles in the synthesis of the fatty acids and the subsequent formation of the acyl-CoAs. For instance, ethylchloroformate is used to form mixed anhydrides of the fatty acids, which are then reacted with CoASH to produce the desired acyl-CoAs. The study also employs various solvents such as methanol, acetonitrile, and tetrahydrofuran, as well as reagents for purification and characterization processes like 2-(2-pyridyl)ethyl-functionalized silica gel for solid-phase extraction and ammonium formate for HPLC elution. The synthesized acyl-CoAs are characterized using techniques such as gas chromatography/mass spectrometry (GC/MS), nuclear magnetic resonance (NMR), and high-performance liquid chromatography with ultraviolet detection and tandem mass spectrometry (HPLC–UV–MS–MS/MS). The purified acyl-CoAs are then used as substrates for measuring acyl-CoA dehydrogenase activities in rat skeletal muscle mitochondria, providing valuable insights into the enzymatic activities related to fatty acid oxidation.

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