Methanone, [2-[[(2,4-dimethoxyphenyl)methyl]amino]-5-methoxyphenyl](3-fluorophen yl)-

Base Information

Chemical Name:Methanone, [2-[[(2,4-dimethoxyphenyl)methyl]amino]-5-methoxyphenyl](3-fluorophen yl)-
CAS No.:849435-47-8
Molecular Formula:C23H22FNO4
Molecular Weight:395.43
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, [2-[[(2,4-dimethoxyphenyl)methyl]amino]-5-methoxyphenyl](3-fluorophen yl)-

Chemical Property:

Purity/Quality:

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Technology Process of Methanone, [2-[[(2,4-dimethoxyphenyl)methyl]amino]-5-methoxyphenyl](3-fluorophen yl)-

There total 1 articles about Methanone, [2-[[(2,4-dimethoxyphenyl)methyl]amino]-5-methoxyphenyl](3-fluorophen yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849435-46-7
(2-amino-5-methoxyphenyl)(3-fluorophenyl)methanone

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 849435-47-8
{2-[(2,4-dimethoxybenzyl)amino]-5-methoxyphenyl}(3-fluorophenyl)methanone

Guidance literature:: With 4 A molecular sieve; sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 3h; Product distribution / selectivity;

Reference yield: 99.0%

: 849435-47-8
{2-[(2,4-dimethoxybenzyl)amino]-5-methoxyphenyl}(3-fluorophenyl)methanone

: 372-09-8
cyanoacetic acid

: 849435-48-9
2-cyano-N-(2,4-dimethoxybenzyl)-N-[2-(3-fluorobenzoyl)-4-methoxyphenyl]acetamide

Guidance literature:: cyanoacetic acid; With phosphorus pentachloride; In dichloromethane; at 20 ℃; for 0.166667h; Heating / reflux;

{2-[(2,4-dimethoxybenzyl)amino]-5-methoxyphenyl}(3-fluorophenyl)methanone; In dichloromethane; for 1.5h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 849435-47-8
{2-[(2,4-dimethoxybenzyl)amino]-5-methoxyphenyl}(3-fluorophenyl)methanone

: 849435-30-9
4-(3-fluorophenyl)-6-methoxy-2-oxo-1,2-dihydroquinoline-3-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphorus pentachloride / dichloromethane / 0.17 h / 20 °C / Heating / reflux

1.2: 1.5 h / Heating / reflux

2.1: sodium methylate / methanol / 0.08 h / Heating / reflux

3.1: dimethylsulfide; trifluoroacetic acid / dichloromethane / 58 h / Heating / reflux

With dimethylsulfide; phosphorus pentachloride; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane;