Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride

Base Information

Chemical Name:Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride
CAS No.:96783-20-9
Molecular Formula:C₁₂H₁₄BrNO*ClH
Molecular Weight:304.614
Hs Code.:
DSSTox Substance ID:DTXSID10914326

Synonyms:Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride;2-Amino-2-(p-bromophenyl)cyclohexanone hydrochloride;2-(p-Bromophenyl)-2-aminocyclohexan-1-one hydrochloride;Cyclohexanone, 2-amino-2-(p-bromophenyl)-, hydrochloride;96783-20-9;C12H14BrNO.ClH;DTXSID10914326;C12-H14-Br-N-O.Cl-H;LS-57264;2-Amino-2-(4-bromophenyl)cyclohexan-1-one--hydrogen chloride (1/1)

Suppliers and Price of Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride

Chemical Property:

Vapor Pressure:6.97E-06mmHg at 25°C
Boiling Point:377°Cat760mmHg
Flash Point:181.8°C
Density:g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:303.00255
Heavy Atom Count:16
Complexity:248

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(C(=O)C1)(C2=CC=C(C=C2)Br)N.Cl

Technology Process of Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride

There total 2 articles about Cyclohexanone, 2-amino-2-(4-bromophenyl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1605-17-0
1-Bromo-4-(1-cyclohexen-1-yl)benzene

: 96783-20-9
2-p-bromophenyl-2-aminocyclohexan-1-one hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 40.8 percent / Na₂CO₃, peracetic acid / CH₂Cl₂ / 4 h / 0 °C

2: 1.) NaN₃, AcOH; 2.) LiAlH₄; 3.) CrO₃, glacial AcOH / 1.) EtOH-water, RT, 6 h; 100 deg C, 10 h; 2.) ether, reflux, 5 h; overnight; 3.) H₂O, 50 deg C, 5 h

With chromium(VI) oxide; peracetic acid; lithium aluminium tetrahydride; sodium azide; sodium carbonate; acetic acid; In dichloromethane;

Reference yield:

: 1605-15-8
1-p-bromophenyl-1,2-epoxycyclohexane

: 1-p-bromophenyl-2-aminocyclohexan-1-ol hydrochloride

: 96783-20-9
2-p-bromophenyl-2-aminocyclohexan-1-one hydrochloride

Guidance literature:: With chromium(VI) oxide; lithium aluminium tetrahydride; sodium azide; acetic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) EtOH-water, RT, 6 h; 100 deg C, 10 h; 2.) ether, reflux, 5 h; overnight; 3.) H₂O, 50 deg C, 5 h;