2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-
CAS No.:79759-77-6
Molecular Formula:C₁₈H₁₃ClN₂O
Molecular Weight:308.767
Hs Code.:
DSSTox Substance ID:DTXSID20229897
Wikidata:Q83110269

Synonyms:BRN 5586840;2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-;79759-77-6;1,3-Dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-2H-benzimidazol-2-one;DTXSID20229897;LS-33320

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-

Chemical Property:

Vapor Pressure:6.66E-10mmHg at 25°C
Boiling Point:494.1°Cat760mmHg
Flash Point:252.6°C
Density:1.357g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:308.0716407
Heavy Atom Count:22
Complexity:443

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)N(C1=O)C3=CC4=CC=CC=C4C=C3

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)-

There total 6 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-naphthalenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.4%

: 79759-76-5
6-Chloro-1-naphthalen-2-yl-1,3-dihydro-benzoimidazol-2-one

: 74-88-4
methyl iodide

: 79759-77-6
5-Chloro-1-methyl-3-naphthalen-2-yl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: With sodium hydroxide; In methanol; for 10h; Ambient temperature;

Reference yield:

: 610-40-2
3,4-dinitro-chlorobenzene

: 79759-77-6
5-Chloro-1-methyl-3-naphthalen-2-yl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 45 percent / ethanol / 13 h / Heating

2: 92 percent / hydrogen / PtO₂ / ethanol / 760 Torr / Ambient temperature

3: 90 percent / xylene / 5 h / Heating

4: 31 percent / EtONa / ethanol / 3 h / Heating

5: 34.4 percent / NaOH / methanol / 10 h / Ambient temperature

With sodium hydroxide; hydrogen; sodium ethanolate; platinum(IV) oxide; In methanol; ethanol; xylene;

Reference yield:

: 79759-02-7
N-(5-chloro-2-nitrophenyl)-N-2-naphthylamine

: 79759-77-6
5-Chloro-1-methyl-3-naphthalen-2-yl-1,3-dihydro-benzoimidazol-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / hydrogen / PtO₂ / ethanol / 760 Torr / Ambient temperature

2: 90 percent / xylene / 5 h / Heating

3: 31 percent / EtONa / ethanol / 3 h / Heating

4: 34.4 percent / NaOH / methanol / 10 h / Ambient temperature

With sodium hydroxide; hydrogen; sodium ethanolate; platinum(IV) oxide; In methanol; ethanol; xylene;