2,2,6,6-Tetramethylpiperidine hydrochloride

Base Information

Chemical Name:2,2,6,6-Tetramethylpiperidine hydrochloride
CAS No.:935-22-8
Molecular Formula:C₉H₂₀N*Cl
Molecular Weight:177.717
Hs Code.:2933399090
DSSTox Substance ID:DTXSID90239448
Mol file:935-22-8.mol

Synonyms:2,2,6,6-Tetramethylpiperidine hydrochloride;935-22-8;TP HCl;Piperidine, 2,2,6,6-tetramethyl-, hydrochloride;2,2,6,6-tetramethylpiperidine;hydrochloride;Tempidine;DTXSID90239448;LS-116193;FT-0691317;2,2,6,6-TETRAMETHYLPIPERIDINEHYDROCHLORIDE

Suppliers and Price of 2,2,6,6-Tetramethylpiperidine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,2,6,6-Tetramethylpiperidine hydrochloride

Chemical Property:

Vapor Pressure:2.73mmHg at 25°C
Melting Point:299-301 °C(lit.)
Boiling Point:157.6°Cat760mmHg
Flash Point:24.4°C
PSA：12.03000
Density:g/cm³
LogP:3.44790
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:177.1284273
Heavy Atom Count:11
Complexity:111

Purity/Quality:: 98% (TLC) ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22
Safety Statements: 36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCCC(N1)(C)C)C.Cl

Technology Process of 2,2,6,6-Tetramethylpiperidine hydrochloride

There total 7 articles about 2,2,6,6-Tetramethylpiperidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 768-66-1
2,2,6,6-tetramethyl-piperidine

: 935-22-8
2,2,6,6-Tetramethylpiperidiniumhydrochlorid

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃;
DOI:10.1002/anie.201507298

Reference yield: 48.0%

: 79855-29-1
dichloro-(2,2,6,6,-tetramethylpiperidino)borane

: 935-22-8
2,2,6,6-Tetramethylpiperidiniumhydrochlorid

Guidance literature:: With Me₃Si-N(CH₃)-SO₂-N(CH₃)-SiMe₃; In toluene; for 10h; Heating;

Reference yield: 48.0%

: 74669-28-6
Me₃Si-N(CH₃)-SO₂-N(CH₃)-SiMe₃

: 79855-29-1
dichloro-(2,2,6,6,-tetramethylpiperidino)borane

: 935-22-8
2,2,6,6-Tetramethylpiperidiniumhydrochlorid

Guidance literature:: In toluene; byproducts: Me3SiCl; under protective gas; reflux of solution (10 h);; evapn. (vacuo); extn. (n-hexane/CH2Cl2); residue was recrystd. (CH2Cl2); elem. anal.; extract contains mixture of two B-compounds; (11)B-NMR;;