L-Phenylalanine, 2-(phenylmethoxy)-N-[(phenylmethoxy)carbonyl]-5-(4,4,5,5-tetramethyl-1 ,3,2-dioxaborolan-2-yl)-, 2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:L-Phenylalanine, 2-(phenylmethoxy)-N-[(phenylmethoxy)carbonyl]-5-(4,4,5,5-tetramethyl-1 ,3,2-dioxaborolan-2-yl)-, 2-(trimethylsilyl)ethyl ester
CAS No.:849814-34-2
Molecular Formula:C35H46BNO7Si
Molecular Weight:631.649
Hs Code.:

L-Phenylalanine,
2-(phenylmethoxy)-N-[(phenylmethoxy)carbonyl]-5-(4,4,5,5-tetramethyl-1
,3,2-dioxaborolan-2-yl)-, 2-(trimethylsilyl)ethyl ester

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Chemical Property of L-Phenylalanine, 2-(phenylmethoxy)-N-[(phenylmethoxy)carbonyl]-5-(4,4,5,5-tetramethyl-1 ,3,2-dioxaborolan-2-yl)-, 2-(trimethylsilyl)ethyl ester

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Technology Process of L-Phenylalanine, 2-(phenylmethoxy)-N-[(phenylmethoxy)carbonyl]-5-(4,4,5,5-tetramethyl-1 ,3,2-dioxaborolan-2-yl)-, 2-(trimethylsilyl)ethyl ester

There total 1 articles about L-Phenylalanine, 2-(phenylmethoxy)-N-[(phenylmethoxy)carbonyl]-5-(4,4,5,5-tetramethyl-1 ,3,2-dioxaborolan-2-yl)-, 2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 616888-59-6
2(S)-benzyloxycarbonylamino-3-(2-benzyloxy-5-iodophenyl)propionic acid (2-trimethylsilyl)ethyl ester

: 73183-34-3
bis(pinacol)diborane

: 849814-34-2
2-(trimethylsilyl)ethyl 2-(benzyloxy)-N-[(benzyloxy)carbonyl]-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-L-phenylalaninate

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 6h;

Reference yield: 86.0%

: 849814-34-2
2-(trimethylsilyl)ethyl 2-(benzyloxy)-N-[(benzyloxy)carbonyl]-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-L-phenylalaninate

: 856222-49-6
methyl 3-bromo-N-(tert-butoxycarbonyl)-6-fluoro-N-methyl-L-phenylalaninate

: 856222-60-1
methyl (2S)-3-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}-4-fluorobiphenyl-3-yl)-2-[(tert-butoxycarbonyl)(methyl)amino]propanoate

Guidance literature:: With caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1-methyl-pyrrolidin-2-one; at 20 - 50 ℃; for 20h;

Reference yield: 83.0%

: 849814-34-2
2-(trimethylsilyl)ethyl 2-(benzyloxy)-N-[(benzyloxy)carbonyl]-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-L-phenylalaninate

: 919988-45-7
methyl 4-(3-bromophenyl)-3-[(tert-butoxycarbonyl)amino]butanoate

: Methyl 4-(4'-(benzyloxy)-3'-{(2S)-2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-[2-(trimethylsilyl)ethoxy]propyl}biphenyl-3-yl)-3-[(tert-butoxycarbonyl)amino]butanoate

Guidance literature:: With caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1-methyl-pyrrolidin-2-one; water; at 50 ℃; for 6h;