(1,2-Dichloro-2-phenylethenyl)benzene

Base Information

• Chemical Name: (1,2-Dichloro-2-phenylethenyl)benzene
• CAS No.: 951-86-0
• Molecular Formula: C14H10Cl2
• Molecular Weight: 249.139
• DSSTox Substance ID: DTXSID801034470
• Nikkaji Number: J14.461D,J7.187K
• Mol file: 951-86-0.mol

Synonyms:1,2-DICHLORO-1,2-DIPHENYLETHENE (TRANS);951-86-0;(1,2-dichloro-2-phenylethenyl)benzene;I+/--Dichlorstilben;SCHEMBL3940726;FTIHFTVXYNBUSM-BUHFOSPRSA-N;Benzene, 1,1'-(1,2-dichloro-1,2-ethenediyl)bis-, (E)-;DTXSID801034470;[(E)-1,2-Dichloro-2-phenylethenyl]benzene #

Chemical Property of (1,2-Dichloro-2-phenylethenyl)benzene

Chemical Property:

• Boiling Point: 337°Cat760mmHg
• Flash Point: 146.1°C
• Density: 1.232g/cm³
• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 248.0159557
• Heavy Atom Count: 16
• Complexity: 220

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=C(C2=CC=CC=C2)Cl)Cl
• Isomeric SMILES: C1=CC=C(C=C1)/C(=C(/C2=CC=CC=C2)\Cl)/Cl

Technology Process of (1,2-Dichloro-2-phenylethenyl)benzene

There total 45 articles about (1,2-Dichloro-2-phenylethenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,1,2,2-tetrachloro-1,2-diphenylethane (13700-81-7) → (E)-1,2-dichlorostilbene (951-86-0)

Guidance literature:

With Co(dmgH)2(S(CH₃)2); In acetone; for 15h;

DOI:10.1016/S0022-328X(00)80133-3

Reference yield: 74.0%

diphenyl acetylene (501-65-5) → (E)-1,2-dichlorostilbene (951-86-0)

Guidance literature:

With hydrogenchloride; iodosylbenzene; In solid; for 0.0833333h; Ambient temperature;

DOI:10.1246/cl.1991.1391

Reference yield: 73.0%

Benzotrichlorid (98-07-7) → (E)-1,2-dichlorostilbene (951-86-0)

Guidance literature:

With zirconium chloride; In tetrahydrofuran; Heating;

DOI:10.1002/cber.19971300903

upstream raw materials:

1,1,2,2-tetrachloro-1,2-diphenylethane

ethylmagnesium bromide

Benzotrichlorid

diphenyl acetylene

Downstream raw materials:

diphenyl acetylene

1,1'-(1,2-ethanediyl)bisbenzene

benzil

valeric acid