Ammonium, (3-(methylcarbamoyloxy)-p-tolyl)trimethyl-, iodide

Base Information

• Chemical Name: Ammonium, (3-(methylcarbamoyloxy)-p-tolyl)trimethyl-, iodide
• CAS No.: 7142-64-5
• Molecular Formula: C12H19N2O2+
• Molecular Weight: 350.1959
• NSC Number: 11847
• Mol file: 7142-64-5.mol

Synonyms:TL-1071;NSC 11847;T-1708;7142-64-5;Ammonium, (3-(methylcarbamoyloxy)-p-tolyl)trimethyl-, iodide;Carbamic acid, methyl-, 5-(trimethylammonio)-o-tolyl ester, iodide;AMMONIUM, (3-HYDROXY-p-TOLYL)TRIMETHYL-, IODIDE, METHYLCARBAMATE;Methiodide of N-methylurethane of 5-dimethylamino-4-isopropyl-o-cresol;Carbamic acid, N-methyl-, 2-methyl-5-dimethylaminophenyl ester, methiodide;NSC11847;NSC-11847;LS-18583;WLN: 1MVOR B1 EK1&1&1 &Q &I;Carbamic acid, 2-methyl-5-(dimethylamino)phenyl ester, methiodide

Chemical Property of Ammonium, (3-(methylcarbamoyloxy)-p-tolyl)trimethyl-, iodide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 350.04913
• Heavy Atom Count: 17
• Complexity: 248

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=C(C=C1)[N+](C)(C)C)OC(=O)NC.[I-]

Technology Process of Ammonium, (3-(methylcarbamoyloxy)-p-tolyl)trimethyl-, iodide

There total 3 articles about Ammonium, (3-(methylcarbamoyloxy)-p-tolyl)trimethyl-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-carbamic acid-(5-dimethylamino-2-methyl-phenyl ester) (24996-52-9) + methyl iodide (74-88-4) → 4,N,N,N-tetramethyl-3-methylcarbamoyloxy-anilinium; iodide (7142-64-5)

Guidance literature:

With acetone;

Reference yield:

N',N',6-trimethylbenzene-1,3-diamine (6370-29-2) → 4,N,N,N-tetramethyl-3-methylcarbamoyloxy-anilinium; iodide (7142-64-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium nitrite; aqueous sulfuric acid / Erhitzen der Diazoniumsalz-Loesung mit Kupfer und wss.Schwefelsaeure

3: 100 °C

With sulfuric acid; sodium nitrite;

Reference yield:

5-Dimethylamino-2-methyl-phenol (56140-38-6) → 4,N,N,N-tetramethyl-3-methylcarbamoyloxy-anilinium; iodide (7142-64-5)

Guidance literature:

Multi-step reaction with 2 steps

2: 100 °C

upstream raw materials:

methyl-carbamic acid-(5-dimethylamino-2-methyl-phenyl ester)

methyl iodide

N',N',6-trimethylbenzene-1,3-diamine

5-Dimethylamino-2-methyl-phenol