Silanol, (3-ethyl-5-phenyl-4-isoxazolyl)dimethyl-

Base Information

Chemical Name:Silanol, (3-ethyl-5-phenyl-4-isoxazolyl)dimethyl-
CAS No.:850131-27-0
Molecular Formula:C13H17NO2Si
Molecular Weight:247.369
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silanol, (3-ethyl-5-phenyl-4-isoxazolyl)dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Silanol, (3-ethyl-5-phenyl-4-isoxazolyl)dimethyl-

There total 2 articles about Silanol, (3-ethyl-5-phenyl-4-isoxazolyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 87710-79-0
methoxy-dimethyl(phenylethynyl)silane

: 108-03-2
1-Nitropropane

: 850131-27-0
3-ethyl-4-(dimethylhydroxysilyl)-5-phenylisoxazole

Guidance literature:: methoxy-dimethyl(phenylethynyl)silane; 1-Nitropropane; With phenyl isocyanate; triethylamine; In toluene; for 6h; Heating;

With acetic acid; In water; acetonitrile; at 20 ℃; for 2h;
DOI:10.1021/jo047755z

Reference yield:

: 87290-97-9
(phenylethynyl)dimethylsilane

: 850131-27-0
3-ethyl-4-(dimethylhydroxysilyl)-5-phenylisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: 70 percent / norbornadiene; palladium chloride / 0.33 h

2.1: phenylisocyanate; triethylamine / toluene / 6 h / Heating

2.2: 49 percent / AcOH / acetonitrile; H₂O / 2 h / 20 °C

With phenyl isocyanate; bicyclo[2.2.1]hepta-2,5-diene; triethylamine; palladium dichloride; In toluene;
DOI:10.1021/jo047755z

Reference yield: 78.0%

: 850131-27-0
3-ethyl-4-(dimethylhydroxysilyl)-5-phenylisoxazole

: 636-98-6
p-nitrobenzene iodide

: 3-ethyl-4-(4-nitrophenyl)-5-phenylisoxazole

Guidance literature:: With copper diacetate; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In toluene; at 40 ℃; for 3h;
DOI:10.1021/jo047755z