Ethanedial, dihydrazone

Base Information

• Chemical Name: Ethanedial, dihydrazone
• CAS No.: 3327-62-6
• Molecular Formula: C2H6N4
• Molecular Weight: 86.0964
• Mol file: 3327-62-6.mol

Synonyms:

Chemical Property of Ethanedial, dihydrazone

Chemical Property:

• Boiling Point: 238.9°Cat760mmHg
• Flash Point: 98.3°C
• Density: 1.28g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanedial, dihydrazone

There total 1 articles about Ethanedial, dihydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Glyoxal (131543-46-9,107-22-2) → glyoxime (557-30-2) + glyoxal bis(hydrazone) (3327-62-6) + Glyoxal monohydrazone monooxime (155944-18-6)

Guidance literature:

With hydroxylamine hydrochloride; hydrazine hydrate; In water; for 4h; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1055/s-1998-1678

Reference yield: 91.0%

glyoxal bis(hydrazone) (3327-62-6) → 1-amino-1,2,3-triazole (584-14-5)

Guidance literature:

With manganese dioxide; In ethanol;

Reference yield: 80.0%

glyoxal bis(hydrazone) (3327-62-6) + phenyl isocyanate (103-71-9) → C16H16N6O2 (80805-29-4)

Guidance literature:

In tetrahydrofuran;

DOI:10.1021/je00028a036

upstream raw materials:

Glyoxal

Downstream raw materials:

C₁₆H₁₆N₆O₂

1-amino-1,2,3-triazole

Refernces