9,9'-Biphenanthrene

Base Information

Chemical Name:9,9'-Biphenanthrene
CAS No.:20532-03-0
Molecular Formula:C28H18
Molecular Weight:354.451
Hs Code.:2902909090
European Community (EC) Number:660-916-7
DSSTox Substance ID:DTXSID30174526
Nikkaji Number:J633.373G
Wikidata:Q83044604
Mol file:20532-03-0.mol

Synonyms:9,9'-Biphenanthrene;9,9'-Biphenanthryl;20532-03-0;DTXSID30174526;UPAPZXUZBAAZCB-UHFFFAOYSA-N;AKOS024433705

Suppliers and Price of 9,9'-Biphenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
9,9'-BIPHENANTHRENE Aldrich
1ea
$ 144.00

Total 3 raw suppliers

Chemical Property of 9,9'-Biphenanthrene

Chemical Property:

Melting Point:188-189 °C(Solv: acetic acid (64-19-7))
Boiling Point:544.4°Cat760mmHg
Flash Point:280.6°C
PSA：0.00000
Density:1.217g/cm³
LogP:7.96640
XLogP3:8.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:354.140850574
Heavy Atom Count:28
Complexity:488

Purity/Quality:

99% ^*data from raw suppliers

9,9'-BIPHENANTHRENE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=C(C3=CC=CC=C23)C4=CC5=CC=CC=C5C6=CC=CC=C64

Technology Process of 9,9'-Biphenanthrene

There total 5 articles about 9,9'-Biphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 68572-87-2
9-phenanthrenylboronic acid

: 20532-03-0
9,9'-biphenanthrene

Guidance literature:: With C₃₄H₅₄N₂O₂; palladium diacetate; potassium carbonate; p-toluenesulfonyl chloride; In water; at 0 - 25 ℃; for 0.25h; Reagent/catalyst; Green chemistry;
DOI:10.1002/aoc.3033

Reference yield: 55.7%

: 85-01-8
phenanthrene

: 20532-03-0
9,9'-biphenanthrene

: 947-72-8
9-chlorophenanthrene

Guidance literature:: With Iodine monochloride; In acetonitrile; for 24h;
DOI:10.1021/jo00103a026

Reference yield:

: potassiumhexacyanoferrate(II) trihydrate

: 573-17-1
9-bromophenanthrene

: 2510-55-6
9-cyanophenanthrene

: 20532-03-0
9,9'-biphenanthrene

Guidance literature:: With [Pd{C₆H₄(CH₂N(CH₂Ph)₂)}(μ-Br)]₂; tetrabutylammomium bromide; potassium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.166667h; Microwave irradiation;
DOI:10.1016/j.tetlet.2011.11.087