Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro-

Base Information

Chemical Name:Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro-
CAS No.:6962-73-8
Molecular Formula:C₉H₁₀ClN
Molecular Weight:167.638
Hs Code.:
NSC Number:54010
DSSTox Substance ID:DTXSID30288071

Synonyms:6962-73-8;Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro-;NSC54010;SCHEMBL679783;DTXSID30288071;NSC-54010;5-chloro-5-cyanobicyclo[2,2,2]oct-2-ene;5-chloro-5-cyanobicyclo[2.2.2]oct-2-ene;2-Chlorobicyclo[2.2.2]oct-5-ene-2-carbonitrile #;6-chloro-bicyclo[2.2.2]oct-7-ene-6-carbonitrile

Suppliers and Price of Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro-

Chemical Property:

Vapor Pressure:0.00371mmHg at 25°C
Boiling Point:280.8°Cat760mmHg
Flash Point:120.2°C
Density:1.19g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:167.0501770
Heavy Atom Count:11
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2C=CC1CC2(C#N)Cl

Technology Process of Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro-

There total 6 articles about Bicyclo[2.2.2]oct-5-ene-2-carbonitrile, 2-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 38258-93-4
5-cyanobicyclo<2.2.2>oct-2-ene

: 6962-73-8
2-chlorobicyclo<2.2.2>oct-5-ene-2-carbonitrile

Guidance literature:: With pyridine; phosphorus pentachloride; In chloroform; for 15h; Reflux;

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 920-37-6
2-Chloroacrylonitrile

: 6962-73-8
2-chlorobicyclo<2.2.2>oct-5-ene-2-carbonitrile

Guidance literature:: With 3,5-dibutyl-4-hydroxytoluene; at 70 ℃; for 40h; Inert atmosphere;

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 6962-73-8
2-chlorobicyclo<2.2.2>oct-5-ene-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / hydroquinone / 18 h / 120 °C

2: 93 percent / PCl₅, pyridine / CHCl₃ / 16 h / Heating

With pyridine; phosphorus pentachloride; hydroquinone; In chloroform;
DOI:10.1021/jo00155a014