Sulfoximine, S-ethyl-S-(4-nitrophenyl)-

Base Information

Chemical Name:Sulfoximine, S-ethyl-S-(4-nitrophenyl)-
CAS No.:851008-74-7
Molecular Formula:C8H10N2O3S
Molecular Weight:214.245
Hs Code.:

Synonyms:

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Chemical Property of Sulfoximine, S-ethyl-S-(4-nitrophenyl)-

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Technology Process of Sulfoximine, S-ethyl-S-(4-nitrophenyl)-

There total 4 articles about Sulfoximine, S-ethyl-S-(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7205-70-1
(R,S)-1-(ethylsulfinyl)-4-nitrobenzene

: 851008-74-7
(R,S)-S-ethyl-S-(4-nitrophenyl)sulfoximide

Guidance literature:: (R,S)-1-(ethylsulfinyl)-4-nitrobenzene; With sodium azide; sulfuric acid; sulfur trioxide; at 45 ℃; for 6h; cooling with ice; Inert atmosphere;

With sodium hydrogencarbonate; In water;

Reference yield:

: 7205-60-9
1-(ethylsulfanyl)-4-nitrobenzene

: 851008-74-7
(R,S)-S-ethyl-S-(4-nitrophenyl)sulfoximide

Guidance literature:: Multi-step reaction with 2 steps

1: periodic acid / iron(III) chloride / acetonitrile / 0.83 h / 20 - 30 °C

2: sodium azide; sulfur trioxide; sulfuric acid / 6 h / 45 °C / cooling with ice; Inert atmosphere

With sodium azide; sulfuric acid; sulfur trioxide; periodic acid; iron(III) chloride; In acetonitrile;

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 851008-74-7
(R,S)-S-ethyl-S-(4-nitrophenyl)sulfoximide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol / 0.25 h / 20 °C / cooling with water

1.2: 20 °C / cooling with water

2.1: periodic acid / iron(III) chloride / acetonitrile / 0.83 h / 20 - 30 °C

3.1: sodium azide; sulfur trioxide; sulfuric acid / 6 h / 45 °C / cooling with ice; Inert atmosphere

With sodium azide; sulfuric acid; sulfur trioxide; periodic acid; sodium hydroxide; iron(III) chloride; In ethanol; acetonitrile;