(R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

Base Information

Chemical Name:(R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide
CAS No.:1223498-63-2
Molecular Formula:C₁₀H₁₁F₃N₂O₂S
Molecular Weight:280.271
Hs Code.:

Synonyms:(R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

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Chemical Property of (R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

Chemical Property:

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Technology Process of (R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

There total 5 articles about (R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1223498-62-1
(R,S)-S-ethyl-S-(4-nitrophenyl)-N-(trifluoroacetyl)sulfoximide

: 1223498-63-2
(R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

Guidance literature:: With hydrogenchloride; titanium(III) chloride; In tetrahydrofuran; at 20 ℃; for 3.5h;
DOI:10.1002/cmdc.201300096

Reference yield:

: 7205-60-9
1-(ethylsulfanyl)-4-nitrobenzene

: 1223498-63-2
(R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

Guidance literature:: Multi-step reaction with 4 steps

1: periodic acid / iron(III) chloride / acetonitrile / 0.83 h / 20 - 30 °C

2: sodium azide; sulfur trioxide; sulfuric acid / 6 h / 45 °C / cooling with ice; Inert atmosphere

3: triethylamine / dichloromethane / 3 h / 10 °C / cooling with ice

4: hydrogenchloride; titanium(III) chloride / water; tetrahydrofuran / 3.5 h / 20 °C / cooling with ice

With hydrogenchloride; sodium azide; titanium(III) chloride; sulfuric acid; sulfur trioxide; periodic acid; triethylamine; iron(III) chloride; In tetrahydrofuran; dichloromethane; water; acetonitrile;

Reference yield:

: 1849-36-1
para-nitrobenzenethiol

: 1223498-63-2
(R,S)-S-(4-aminophenyl)-S-ethyl-N-(trifluoroacetyl)sulfoximide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / ethanol / 0.25 h / 20 °C / cooling with water

1.2: 20 °C / cooling with water

2.1: periodic acid / iron(III) chloride / acetonitrile / 0.83 h / 20 - 30 °C

3.1: sodium azide; sulfur trioxide; sulfuric acid / 6 h / 45 °C / cooling with ice; Inert atmosphere

4.1: triethylamine / dichloromethane / 3 h / 10 °C / cooling with ice

5.1: hydrogenchloride; titanium(III) chloride / water; tetrahydrofuran / 3.5 h / 20 °C / cooling with ice

With hydrogenchloride; sodium azide; titanium(III) chloride; sulfuric acid; sulfur trioxide; periodic acid; triethylamine; sodium hydroxide; iron(III) chloride; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;