3-{[3-(chlorosulfonyl)phenyl]sulfonyl}benzenesulfonyl chloride

Base Information

• Chemical Name: 3-{[3-(chlorosulfonyl)phenyl]sulfonyl}benzenesulfonyl chloride
• CAS No.: 7357-41-7
• Molecular Formula: C12H8 Cl2 O6 S3
• Molecular Weight: 415.296
• Mol file: 7357-41-7.mol

Synonyms:Benzenesulfonylchloride, 3,3'-sulfonyldi- (6CI,7CI,8CI); Diphenyl sulfone-3,3'-disulfonylchloride; NSC 59822

Chemical Property of 3-{[3-(chlorosulfonyl)phenyl]sulfonyl}benzenesulfonyl chloride

Chemical Property:

• Boiling Point: 617.8oC at 760 mmHg
• Flash Point: 327.4oC
• PSA: 127.56000
• Density: 1.653g/cm3
• LogP: 5.61680

Purity/Quality:

99%min ^*data from raw suppliers

3,3'-DICHLOROSULFONYLDIPHENYLSULFONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Diphenyl Sulfone-3,3''-disulfonyl Chloride is the derivative of 4,4’-Dichlorodiphenyl Sulfone (D434165), which is an antibacterial used in the treatment of dermatitis herpetiformis.

Technology Process of 3-{[3-(chlorosulfonyl)phenyl]sulfonyl}benzenesulfonyl chloride

There total 3 articles about 3-{[3-(chlorosulfonyl)phenyl]sulfonyl}benzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

diphenyl sulphone (127-63-9) → 3,3'-sulfonyldi(benzenesulfonyl chloride) (7357-41-7)

Guidance literature:

With chlorosulfonic acid; potassium chloride; at 130 ℃;

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → benzene-1,3-disulfonyl chloride (585-47-7) + 3,3'-sulfonyldi(benzenesulfonyl chloride) (7357-41-7)

Guidance literature:

With chlorosulfonic acid; sulfuric acid; sulfur trioxide;

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 3,3'-sulfonyldi(benzenesulfonyl chloride) (7357-41-7)

Guidance literature:

With chlorosulphuric acid; beim Erhitzen des Reaktionsgemisches mit Chloroschwefelsaeure auf 150grad;

upstream raw materials:

benzene

diphenyl sulphone

Downstream raw materials:

C₂₆H₂₄N₂O₆S₃

C₂₀H₂₈N₂O₆S₃

3,3'-bis(2-phenylprop-2-en-1-ylsulfonyl)diphenyl sulfone

3,3'-sulfonyl-bis-benzenesulfonic acid dianilide

Refernces

• 1、 Yablonskii,Tarasov,Moskvichev. "Synthesis of new sulfonyl chlorides on the basis of substituted diphenyl sulfones". . p. 60 - 63. Retrieved 2007/10/03.
• 2、 Moskvichev, Yu. A.,Sapunov, V. A.,Mironov, G. S.. "Synthesis of aromatic sulfonyl chlorides - monomers for sulfur-containing polycondensation polymers". . p. 1264 - 1268. Retrieved 2007/10/02.