1-Butanone, 1-[(1R,4R)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-2,2-dimethyl-1 ,3-dioxolan-4-yl]-4-hydroxy-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)meth oxy]-

Base Information

Chemical Name:1-Butanone, 1-[(1R,4R)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-2,2-dimethyl-1 ,3-dioxolan-4-yl]-4-hydroxy-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)meth oxy]-
CAS No.:851370-29-1
Molecular Formula:C29H43N3O6
Molecular Weight:529.677
Hs Code.:

1-Butanone,
1-[(1R,4R)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-2,2-dimethyl-1
,3-dioxolan-4-yl]-4-hydroxy-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)meth
oxy]-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Butanone, 1-[(1R,4R)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-2,2-dimethyl-1 ,3-dioxolan-4-yl]-4-hydroxy-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)meth oxy]-

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Technology Process of 1-Butanone, 1-[(1R,4R)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-2,2-dimethyl-1 ,3-dioxolan-4-yl]-4-hydroxy-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)meth oxy]-

There total 16 articles about 1-Butanone, 1-[(1R,4R)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-2,2-dimethyl-1 ,3-dioxolan-4-yl]-4-hydroxy-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)meth oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Toluene-4-sulfonic acid (2R,3S)-4-{(1R,4R)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-1-[4-(4-methoxy-benzyloxy)-butyryl]-cyclohex-2-enyl}-2,3-dimethyl-butyl ester

: 851370-29-1
1-[(1R,4R)-1-((2S,3R)-4-Azido-2,3-dimethyl-butyl)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-cyclohex-2-enyl]-4-(4-methoxy-benzyloxy)-butan-1-one

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 70 ℃; for 4h;
DOI:10.1021/ol050321l

Reference yield:

: 851370-40-6
1-[(1R,4R)-4-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-1-((2S,3R)-4-hydroxy-2,3-dimethyl-butyl)-cyclohex-2-enyl]-4-(4-methoxy-benzyloxy)-butan-1-one

: 851370-29-1
1-[(1R,4R)-1-((2S,3R)-4-Azido-2,3-dimethyl-butyl)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-cyclohex-2-enyl]-4-(4-methoxy-benzyloxy)-butan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N

2: NaN₃ / dimethylformamide

With sodium azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.08.083

Reference yield:

: 851370-27-9
2,2-Dimethyl-propionic acid (2R,3S)-4-{(1R,4R)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-1-[4-(4-methoxy-benzyloxy)-butyryl]-cyclohex-2-enyl}-2,3-dimethyl-butyl ester

: 851370-29-1
1-[(1R,4R)-1-((2S,3R)-4-Azido-2,3-dimethyl-butyl)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-cyclohex-2-enyl]-4-(4-methoxy-benzyloxy)-butan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: MeONa / methanol

2: Et₃N

3: NaN₃ / dimethylformamide

With sodium azide; sodium methylate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.08.083