1-Butanone, 1-[(1R,4R)-4-(acetyloxy)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)- 2,2-dimethyl-1,3-dioxolan-4-yl]-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl) methoxy]-

Base Information

Chemical Name:1-Butanone, 1-[(1R,4R)-4-(acetyloxy)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)- 2,2-dimethyl-1,3-dioxolan-4-yl]-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl) methoxy]-
CAS No.:851370-30-4
Molecular Formula:C31H45N3O7
Molecular Weight:571.714
Hs Code.:

1-Butanone,
1-[(1R,4R)-4-(acetyloxy)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)-
2,2-dimethyl-1,3-dioxolan-4-yl]-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl)
methoxy]-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Butanone, 1-[(1R,4R)-4-(acetyloxy)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)- 2,2-dimethyl-1,3-dioxolan-4-yl]-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl) methoxy]-

Chemical Property:

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Technology Process of 1-Butanone, 1-[(1R,4R)-4-(acetyloxy)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)- 2,2-dimethyl-1,3-dioxolan-4-yl]-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl) methoxy]-

There total 17 articles about 1-Butanone, 1-[(1R,4R)-4-(acetyloxy)-1-[(2S,3R)-4-azido-2,3-dimethylbutyl]-4-[(4S)- 2,2-dimethyl-1,3-dioxolan-4-yl]-2-cyclohexen-1-yl]-4-[(4-methoxyphenyl) methoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 851370-29-1
1-[(1R,4R)-1-((2S,3R)-4-Azido-2,3-dimethyl-butyl)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-cyclohex-2-enyl]-4-(4-methoxy-benzyloxy)-butan-1-one

: 108-24-7
acetic anhydride

: 851370-30-4
Acetic acid (1R,4R)-4-((2S,3R)-4-azido-2,3-dimethyl-butyl)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-[4-(4-methoxy-benzyloxy)-butyryl]-cyclohex-2-enyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 4.5h; Heating;
DOI:10.1021/ol050321l

Reference yield:

: 851370-40-6
1-[(1R,4R)-4-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-1-((2S,3R)-4-hydroxy-2,3-dimethyl-butyl)-cyclohex-2-enyl]-4-(4-methoxy-benzyloxy)-butan-1-one

: 851370-30-4
Acetic acid (1R,4R)-4-((2S,3R)-4-azido-2,3-dimethyl-butyl)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-[4-(4-methoxy-benzyloxy)-butyryl]-cyclohex-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N

2: NaN₃ / dimethylformamide

3: DMAP

With dmap; sodium azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.08.083

Reference yield:

: 851370-27-9
2,2-Dimethyl-propionic acid (2R,3S)-4-{(1R,4R)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-hydroxy-1-[4-(4-methoxy-benzyloxy)-butyryl]-cyclohex-2-enyl}-2,3-dimethyl-butyl ester

: 851370-30-4
Acetic acid (1R,4R)-4-((2S,3R)-4-azido-2,3-dimethyl-butyl)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-4-[4-(4-methoxy-benzyloxy)-butyryl]-cyclohex-2-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: MeONa / methanol

2: Et₃N

3: NaN₃ / dimethylformamide

4: DMAP

With dmap; sodium azide; sodium methylate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.08.083