Butanoic acid, 3-hydroxy-4-(phenylseleno)-, ethyl ester, (3S)-

Base Information

Chemical Name:Butanoic acid, 3-hydroxy-4-(phenylseleno)-, ethyl ester, (3S)-
CAS No.:851387-84-3
Molecular Formula:C12H16O3Se
Molecular Weight:287.217
Hs Code.:

Synonyms:

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Chemical Property of Butanoic acid, 3-hydroxy-4-(phenylseleno)-, ethyl ester, (3S)-

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Technology Process of Butanoic acid, 3-hydroxy-4-(phenylseleno)-, ethyl ester, (3S)-

There total 1 articles about Butanoic acid, 3-hydroxy-4-(phenylseleno)-, ethyl ester, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1666-13-3
diphenyl diselenide

: 10488-69-4,86728-85-0,87068-18-6,90866-33-4
ethyl (S)-4-chloro-3-hydroxybutanoate

: 851387-84-3
ethyl (3S)-3-hydroxy-4-(phenylseleno)butanoate

Guidance literature:: diphenyl diselenide; With sodium hydride; In tetrahydrofuran; for 2h; Heating;

ethyl (S)-4-chloro-3-hydroxybutanoate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 40 ℃; for 36h;
DOI:10.1055/s-2005-861783

Reference yield: 88.0%

: 851387-84-3
ethyl (3S)-3-hydroxy-4-(phenylseleno)butanoate

: 4461-33-0
benzoyl isocyanate

: 851387-85-4
ethyl (3S)-3-{[(benzoylamino)carbonyl]oxy}-4-(phenylseleno)butanoate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1055/s-2005-861783

Reference yield:

: 851387-84-3
ethyl (3S)-3-hydroxy-4-(phenylseleno)butanoate

: 851387-86-5
ethyl [(5S)-3-benzoyl-2-oxo-1,3-oxazolidin-5-yl]acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / CH₂Cl₂ / 20 °C

2: potassium hydrogenphosphate; m-chloroperoxybenzoic acid / tetrahydrofuran / 4 h / 0 - 20 °C

3: K₂CO₃ / acetone / 20 h / 20 °C

With dipotassium hydrogenphosphate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1055/s-2005-861783