Benzene, 2-bromo-1,3-bis[(4-methylphenoxy)methyl]-

Base Information

Chemical Name:Benzene, 2-bromo-1,3-bis[(4-methylphenoxy)methyl]-
CAS No.:851527-27-0
Molecular Formula:C22H21BrO2
Molecular Weight:397.312
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 2-bromo-1,3-bis[(4-methylphenoxy)methyl]-

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Technology Process of Benzene, 2-bromo-1,3-bis[(4-methylphenoxy)methyl]-

There total 1 articles about Benzene, 2-bromo-1,3-bis[(4-methylphenoxy)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 106-44-5
p-cresol

: 25006-88-6
2-bromo-1,3-bis(bromomethyl)benzene

: 851527-27-0
2,6-bis(p-methylphenoxymethyl)bromobenzene

Guidance literature:: With potassium carbonate; In acetone; for 23h; Heating;
DOI:10.1021/ja043802t

Reference yield: 58.0%

: 851527-27-0
2,6-bis(p-methylphenoxymethyl)bromobenzene

: 119-61-9
benzophenone

: 851527-29-2
diphenyl[2,6-bis(p-methylphenoxymethyl)phenyl]methanol

Guidance literature:: 2,6-bis(p-methylphenoxymethyl)bromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

benzophenone; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/ja043802t

Reference yield: 58.0%

: 851527-27-0
2,6-bis(p-methylphenoxymethyl)bromobenzene

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: Co(CH₃C₆H₄OCH₂C₆H₃CH₂OC₆H₄CH₃)3

Guidance literature:: With n-BuLi; In tetrahydrofuran; hexane; under N2 atm. to soln. 1-bromo-2-(p-tolyloxymethyl)benzene in THF n-BuLiin hexane was added at -78°C, stirred for 1 h and transferred to suspn. Cocl2 in THF at room temp., stirred overnight at room temp.; soln. was filtered through Celite, solvent was evapd., residue was dissolved in CH2Cl2, filtered through alumina and evapd., purification by GPC(ClCH2CH2Cl); elem. anal.;
DOI:10.1016/j.jorganchem.2006.08.100