3-chloro-2-(1-ethoxyethoxy)propyl acetate

Base Information

• Chemical Name: 3-chloro-2-(1-ethoxyethoxy)propyl acetate
• CAS No.: 85328-35-4
• Molecular Formula: C9H17ClO4
• Molecular Weight: 224.68200
• Hs Code.: 2915390090
• Mol file: 85328-35-4.mol

Synonyms:m-ClC6H4-OTf;m-chlorophenyl triflate;3-chlorophenyl trifluoromethanesulfonate;3-chloro-1-trifluoromethanesulfonyloxybenzene;Methanesulfonic acid,trifluoro-,3-chlorophenyl ester;

Chemical Property of 3-chloro-2-(1-ethoxyethoxy)propyl acetate

Chemical Property:

• PSA: 44.76000
• LogP: 1.55600

Purity/Quality:

[3-Chloro-2-(1-ethoxyethoxy)propyl]acetate 94% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-chloro-2-(1-ethoxyethoxy)propyl acetate

There total 1 articles about 3-chloro-2-(1-ethoxyethoxy)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-chloro-2-hydroxy-1-propyl acetate (24573-30-6) + ethyl vinyl ether (109-92-2,25104-37-4) → 3-Chloro-2-(1-ethoxyethoxy)-1-propyl acetate (85328-35-4)

Guidance literature:

With toluene-4-sulfonic acid; at 35 - 45 ℃; for 20h;

Reference yield: 62.4%

3-Chloro-2-(1-ethoxyethoxy)-1-propyl acetate (85328-35-4) → 3-(1-Ethoxyethoxy)oxetane (85328-36-5)

Guidance literature:

With sodium hydroxide; at 110 ℃; for 7h; Reagent/catalyst; Large scale;

upstream raw materials:

3-chloro-2-hydroxy-1-propyl acetate

ethyl vinyl ether

Downstream raw materials:

3-(1-Ethoxyethoxy)oxetane

Refernces

• 1、 -. "A method for synthesis of oxetane butanone (by machine translation)". Paragraph 0027; 0031; 0035. . Retrieved 2019/03/26.
• 2、 Zhao, Yichao,Wang, Wen,Li, Jian,Wang, Feng,Zheng, Xiufang,Yun, Hongying,Zhao, Weili,Dong, Xiaochun. "FeCl3/pyridine: Dual-activation in opening of epoxide with carboxylic acid under solvent free condition". supporting information. p. 5849 - 5852. Retrieved 2013/10/21.