Silane, [[(1E)-1,2-dibromo-1,2-digermenediyl]bis[[5-[tris(trimethylsilyl)methyl]-2, 1,3-benzenetriyl]dimethylidyne]]octakis[trimethyl-

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Chemical Name:Silane, [[(1E)-1,2-dibromo-1,2-digermenediyl]bis[[5-[tris(trimethylsilyl)methyl]-2, 1,3-benzenetriyl]dimethylidyne]]octakis[trimethyl-
CAS No.:857444-41-8
Molecular Formula:C60H134Br2Ge2Si14
Molecular Weight:1553.91
Hs Code.:

Silane,
[[(1E)-1,2-dibromo-1,2-digermenediyl]bis[[5-[tris(trimethylsilyl)methyl]-2,
1,3-benzenetriyl]dimethylidyne]]octakis[trimethyl-

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Chemical Property of Silane, [[(1E)-1,2-dibromo-1,2-digermenediyl]bis[[5-[tris(trimethylsilyl)methyl]-2, 1,3-benzenetriyl]dimethylidyne]]octakis[trimethyl-

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Technology Process of Silane, [[(1E)-1,2-dibromo-1,2-digermenediyl]bis[[5-[tris(trimethylsilyl)methyl]-2, 1,3-benzenetriyl]dimethylidyne]]octakis[trimethyl-

There total 1 articles about Silane, [[(1E)-1,2-dibromo-1,2-digermenediyl]bis[[5-[tris(trimethylsilyl)methyl]-2, 1,3-benzenetriyl]dimethylidyne]]octakis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: dibromogermane dioxane

: (E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 857444-41-8
(E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

Guidance literature:: With t-BuLi; In tetrahydrofuran; pentane; (Ar); soln. of BuLi in pentane was added to soln. of Si compd. in THF at-78°C; mixt. was stirred for 30 min; Ge compd. was added at -78. degree.C; stirred for 30 min at -78°C; soln. was warmed to room temp.; solvent removed (vac.); hexane added; filtered through Celite; filtrate concd. at -40°C; recrystd. (hexane); elem. anal.;
DOI:10.1021/om050129n

Reference yield: 99.0%

: 857444-41-8
(E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 876941-91-2
1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

Guidance literature:: With KC₈; In benzene; under Ar atm. to soln. dibromodigermene in C6H6 was added KC8 at room temp., mixt. was stirred for 12 h; mixt. was evapd. in vac., hexane was added to residue, suspn. was filtered, filtrate was condensed, recrystd. from hexane; elem. anal.;
DOI:10.1021/ja057205y

Reference yield: 94.0%

: 10544-50-0
sulfur

: 857444-41-8
(E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 857444-53-2
cis-2,4-dibromo-2,4-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)-1,3,2,4-dithiadigermetane

Guidance literature:: In toluene; (Ar); S8 was added to soln. of Ge compd. in toluene at -78°C; mixt. was stirred at -78°C for 1 h; warmed to room temp. during 12 h; filtered; chromd.; elem. anal.;
DOI:10.1021/om050129n