1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

Base Information

Chemical Name:1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne
CAS No.:876941-91-2
Molecular Formula:C₆₀H₁₃₄Ge₂Si₁₄
Molecular Weight:1394.1
Hs Code.:

Synonyms:1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

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Technology Process of 1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

There total 3 articles about 1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 857444-41-8
(E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 876941-91-2
1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

Guidance literature:: With KC₈; In benzene; under Ar atm. to soln. dibromodigermene in C6H6 was added KC8 at room temp., mixt. was stirred for 12 h; mixt. was evapd. in vac., hexane was added to residue, suspn. was filtered, filtrate was condensed, recrystd. from hexane; elem. anal.;
DOI:10.1021/ja057205y