Methanaminium, N-methyl-N-(3-phenyl-2-propenylidene)-, (E)-,perchlorate

Base Information

• Chemical Name: Methanaminium, N-methyl-N-(3-phenyl-2-propenylidene)-, (E)-,perchlorate
• CAS No.: 86119-07-5
• Molecular Formula: C11H14N.ClO4
• Molecular Weight: 259.689

Synonyms:Methanaminium, N-methyl-N-(3-phenyl-2-propenylidene)-, (E)-,perchlorate

Chemical Property of Methanaminium, N-methyl-N-(3-phenyl-2-propenylidene)-, (E)-,perchlorate

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of Methanaminium, N-methyl-N-(3-phenyl-2-propenylidene)-, (E)-,perchlorate

There total 2 articles about Methanaminium, N-methyl-N-(3-phenyl-2-propenylidene)-, (E)-,perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(E)-3-phenylpropenal (14371-10-9) + dimethylammonium perchlorate → e-N,N-dimethyl-3-phenyl-2-propylideniminium perchlorate (86119-07-5)

Guidance literature:

In methanol;

DOI:10.1021/ja00353a031

Reference yield:

(E)-3-phenylpropenal (14371-10-9) + dimethylammonium perchlorate (14488-49-4) → e-N,N-dimethyl-3-phenyl-2-propylideniminium perchlorate (86119-07-5)

Guidance literature:

DOI:10.1007/BF01185719

Reference yield: 83.0%

e-N,N-dimethyl-3-phenyl-2-propylideniminium perchlorate (86119-07-5) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 3,3-diphenylpropanal (4279-81-6)

Guidance literature:

With trifluorormethanesulfonic acid; at 23 ℃; for 24h;

DOI:10.1021/ja00004a044

upstream raw materials:

(E)-3-phenylpropenal

dimethylammonium perchlorate

Downstream raw materials:

Dimethyl-((Z)-3-phenyl-allylidene)-ammonium

3,3-diphenylpropanal

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