1,3,5-Benzenetricarbonyl trichloride, 2,4,6-tribromo-

Base Information

• Chemical Name: 1,3,5-Benzenetricarbonyl trichloride, 2,4,6-tribromo-
• CAS No.: 86216-69-5
• Molecular Formula: C9Br3Cl3O3
• Molecular Weight: 502.168
• Mol file: 86216-69-5.mol

Synonyms:

Chemical Property of 1,3,5-Benzenetricarbonyl trichloride, 2,4,6-tribromo-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-Benzenetricarbonyl trichloride, 2,4,6-tribromo-

There total 4 articles about 1,3,5-Benzenetricarbonyl trichloride, 2,4,6-tribromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,4,6-tribromo-1,3,5-benzene tricarboxylic acid (86216-68-4) → 2,4,6-tribromo-1,3,5-trisbenzoyl chloride (86216-69-5)

Guidance literature:

In N-methyl-acetamide; thionyl chloride;

Reference yield:

1,3,5-tris(bromo)-2,4,6-tris(bromomethyl) benzene (29165-34-2) → 2,4,6-tribromo-1,3,5-trisbenzoyl chloride (86216-69-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / AcOH / 12 h / Heating

2: aq. NaOH; KMnO₄ / 12 h / Heating

3: SOCl₂ / 12 h / Heating

With sodium hydroxide; potassium permanganate; thionyl chloride; acetic acid;

DOI:10.1021/ja034783a

Reference yield:

(2,4,6-tribromobenzene-1,3,5-triyl)tris(methylene) triacetate (467420-07-1) → 2,4,6-tribromo-1,3,5-trisbenzoyl chloride (86216-69-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH; KMnO₄ / 12 h / Heating

2: SOCl₂ / 12 h / Heating

With sodium hydroxide; potassium permanganate; thionyl chloride;

DOI:10.1021/ja034783a

upstream raw materials:

2,4,6-tribromo-1,3,5-benzene tricarboxylic acid

1,3,5-tris(bromo)-2,4,6-tris(bromomethyl) benzene

(2,4,6-tribromobenzene-1,3,5-triyl)tris(methylene) triacetate

1,3,5-tribromo-2,4,6-tris(hydroxymethyl)benzene

Downstream raw materials:

1,3,5-tribromo-2,4,6-tricyanobenzene

2,4,6-trisphenylethynylbenzene-1,3,5-tricarboxylic acid trimethyl ester

2,4,6-tribromobenzene-1,3,5-tricarboxylic acid trimethyl ester