1,3,5-Benzenetrimethanol, 2,4,6-tribromo-

Base Information

• Chemical Name: 1,3,5-Benzenetrimethanol, 2,4,6-tribromo-
• CAS No.: 191529-08-5
• Molecular Formula: C9H9Br3O3
• Molecular Weight: 404.881
• Mol file: 191529-08-5.mol

Synonyms:1,3,5-Benzenetrimethanol,2,4,6-tribromo;1,3,5-tribromo-2,4,6-trihydroxymethyl-benzene;1,3,5-tribromo-2,4,6-tris(hydroxymethyl)benzene;

Chemical Property of 1,3,5-Benzenetrimethanol, 2,4,6-tribromo-

Chemical Property:

• Boiling Point: 536.2±45.0 °C(Predicted)
• PKA: 12.71±0.10(Predicted)
• PSA: 60.69000
• Density: 2.256±0.06 g/cm3(Predicted)
• LogP: 2.45100

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,5-Benzenetrimethanol, 2,4,6-tribromo-

There total 6 articles about 1,3,5-Benzenetrimethanol, 2,4,6-tribromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(2,4,6-tribromobenzene-1,3,5-triyl)tris(methylene) triacetate (467420-07-1) → 1,3,5-tribromo-2,4,6-tris(hydroxymethyl)benzene (191529-08-5)

Guidance literature:

With potassium hydroxide; In water; for 24h; Heating;

DOI:10.1021/ol027482z

Reference yield: 97.0%

1,3,5-tris(bromo)-2,4,6-tris(bromomethyl) benzene (29165-34-2) → 1,3,5-tribromo-2,4,6-tris(hydroxymethyl)benzene (191529-08-5)

Guidance literature:

1,3,5-tris(bromo)-2,4,6-tris(bromomethyl) benzene; With potassium acetate; In N,N-dimethyl-formamide; at 80 ℃;

With potassium hydroxide; In water; at 90 ℃;

DOI:10.1021/acs.orglett.8b03099

Reference yield: 96.8%

2,4,6-tribromomesitylene (608-72-0) + potassium acetate (127-08-2) → 1,3,5-tribromo-2,4,6-tris(hydroxymethyl)benzene (191529-08-5)

Guidance literature:

2,4,6-tribromomesitylene; With bromine; In dichloromethane; for 10h; Heating;

potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 20h;

With potassium hydroxide; In water; at 90 ℃; for 22h; Further stages.;

DOI:10.1021/ol027482z

upstream raw materials:

(2,4,6-tribromobenzene-1,3,5-triyl)tris(methylene) triacetate

2,4,6-tribromomesitylene

potassium acetate

1,3,5-tris(bromo)-2,4,6-tris(bromomethyl) benzene

Downstream raw materials:

2,4,6-tribromo-1,3,5-benzenetricarboxaldehyde

2,4,6-tris[(trimethylsilyl)ethynyl]-1,3,5-benzenetricarbaldehyde

1,3,5-tris(2,2-dibromo-1-ethenyl)-2,4,6-tris[(trimethylsilyl)ethynyl]benzene

C₁₈H₃₀O₃S₃