N-(4-Amino-2,5-diethoxyphenyl)benzamide

Base Information

• Chemical Name: N-(4-Amino-2,5-diethoxyphenyl)benzamide
• CAS No.: 120-00-3
• Molecular Formula: C17H20N2O3
• Molecular Weight: 300.357
• Hs Code.: 29242998
• European Community (EC) Number: 204-363-8
• NSC Number: 37184
• UNII: 9FB70C7GDI
• DSSTox Substance ID: DTXSID8059504
• Nikkaji Number: J218.149E
• Wikidata: Q27272487
• Mol file: 120-00-3.mol

Synonyms:benzenediazonium, 4-(benzoylamino)-2,5-diethoxy-;Echtblausalz;fast blue 2B salt;Fast Blue BB;Fast Blue BB hexafluorophosphate;Fast Blue BB salt;Fast Blue BB tetrachlorozincate (2:1);Fast blue BBN

Chemical Property of N-(4-Amino-2,5-diethoxyphenyl)benzamide

Chemical Property:

• Appearance/Colour: grey to brown powder or chunks
• Vapor Pressure: 8.74E-07mmHg at 25°C
• Melting Point: 98-100 °C
• Refractive Index: 1.613
• Boiling Point: 405.472 °C at 760 mmHg
• PKA: 12.12±0.70(Predicted)
• Flash Point: 199.023 °C
• PSA: 73.58000
• Density: 1.194 g/cm³
• LogP: 3.97270
• Storage Temp.: 2-8°C
• Solubility.: Chloroform (Slightly), Methanol (Slightly)
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 300.14739250
• Heavy Atom Count: 22
• Complexity: 345

Purity/Quality:

99% ^*data from raw suppliers

FastBlueBB ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi,Xn
• Hazard Codes: Xn,Xi
• Statements: 22-36/37/38-41-37/38
• Safety Statements: 37/39-26-36/37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCOC1=CC(=C(C=C1N)OCC)NC(=O)C2=CC=CC=C2
• Uses: Fast Blue BB is a component used in assays that detect virus in clinical specimen. It is also used in test kits that detect micro-organisms infection. Dyes and metabolites.

Technology Process of N-(4-Amino-2,5-diethoxyphenyl)benzamide

There total 1 articles about N-(4-Amino-2,5-diethoxyphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid-(2,5-diethoxy-4-nitro-anilide) (135-41-1) → 1-amino-4-benzoylamino-2,5-diethoxy-benzene (120-00-3)

Guidance literature:

With hydrogenchloride; iron;

Reference yield: 81.0%

1-amino-4-benzoylamino-2,5-diethoxy-benzene (120-00-3) + 6-((2S,3R,4R,5S,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-yl)-hexanoic acid → 1,2,3,4-tetra-O-acetyl-10-(4-benzamido-2,5-diethyloxyphenylaminocarbonyl)-6,7,8,9,10-pentadeoxy-α-L-galacto-decopyranose

Guidance literature:

With 4 A molecular sieve; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1081/CAR-100108277

Reference yield: 81.0%

1-amino-4-benzoylamino-2,5-diethoxy-benzene (120-00-3) + 6-((2S,3R,4R,5S,6R)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-yl)-hexanoic acid → 1,2,3,4-tetra-O-acetyl-10-(4-benzamido-2,5-diethyloxyphenylaminocarbonyl)-6,7,8,9,10-pentadeoxy-β-L-galacto-decopyranose

Guidance literature:

With 4 A molecular sieve; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1081/CAR-100108277

upstream raw materials:

benzoic acid-(2,5-diethoxy-4-nitro-anilide)

Downstream raw materials:

C₃₈H₃₁N₃O₆