Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]-

Base Information

Chemical Name:Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]-
CAS No.:86801-13-0
Molecular Formula:C₁₁H₁₁ClN₂O₄
Molecular Weight:270.672
Hs Code.:
DSSTox Substance ID:DTXSID30395138

Synonyms:86801-13-0;Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]-;DTXSID30395138

Suppliers and Price of Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]-

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:270.0407345
Heavy Atom Count:18
Complexity:346

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=NNC1=CC=CC=C1C(=O)O)Cl

Technology Process of Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]-

There total 1 articles about Benzoic acid, 2-[(1-chloro-2-ethoxy-2-oxoethylidene)hydrazino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 86801-13-0
C₁₁H₁₁ClN₂O₄

Guidance literature:: With sodium acetate; Multistep reaction; 1) diazotization 2) ethanol, standing overnight in ice box;

Reference yield:

: 86801-13-0
C₁₁H₁₁ClN₂O₄

: (4-Imino-1-phenyl-6-thioxo-1,4,6,7-tetrahydro-pyrazolo[3,4-d][1,3]thiazin-3-yl)-phenyl-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: Sodium, ethanol / 24 h / Ambient temperature

2: Sodium methoxide / dimethylformamide / 45 h / Heating

With ethanol; sodium methylate; sodium; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210425

Reference yield:

: 86801-13-0
C₁₁H₁₁ClN₂O₄

: 93745-35-8
2-Phenyl-8-p-tolyl-2,5-dihydro-3H-1,2,3,5,6,7-hexaaza-acenaphthylen-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: Sodium, ethanol / 24 h / Ambient temperature

2: Hydrazine hydrate / 4 h / Heating

3: dimethylformamide

With ethanol; sodium; hydrazine hydrate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210425