1,4,7,10-Tetraazacyclododecane-1,4,7-tricarboxylic acid, 10-[[5-[(dimethylamino)sulfonyl]-8-[(phenylsulfonyl)oxy]-2-quinolinyl]meth yl]-, tris(1,1-dimethylethyl) ester

Base Information

Chemical Name:1,4,7,10-Tetraazacyclododecane-1,4,7-tricarboxylic acid, 10-[[5-[(dimethylamino)sulfonyl]-8-[(phenylsulfonyl)oxy]-2-quinolinyl]meth yl]-, tris(1,1-dimethylethyl) ester
CAS No.:869984-55-4
Molecular Formula:C41H60N6O11S2
Molecular Weight:877.093
Hs Code.:

1,4,7,10-Tetraazacyclododecane-1,4,7-tricarboxylic acid,
10-[[5-[(dimethylamino)sulfonyl]-8-[(phenylsulfonyl)oxy]-2-quinolinyl]meth
yl]-, tris(1,1-dimethylethyl) ester

Synonyms:

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Chemical Property of 1,4,7,10-Tetraazacyclododecane-1,4,7-tricarboxylic acid, 10-[[5-[(dimethylamino)sulfonyl]-8-[(phenylsulfonyl)oxy]-2-quinolinyl]meth yl]-, tris(1,1-dimethylethyl) ester

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,4,7,10-Tetraazacyclododecane-1,4,7-tricarboxylic acid, 10-[[5-[(dimethylamino)sulfonyl]-8-[(phenylsulfonyl)oxy]-2-quinolinyl]meth yl]-, tris(1,1-dimethylethyl) ester

There total 4 articles about 1,4,7,10-Tetraazacyclododecane-1,4,7-tricarboxylic acid, 10-[[5-[(dimethylamino)sulfonyl]-8-[(phenylsulfonyl)oxy]-2-quinolinyl]meth yl]-, tris(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 869984-54-3
8-benzenesulfonyloxy-2-bromomethyl-5-N,N-dimethylaminosulfonylquinoline

: 913528-02-6
1,4,7-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

: 869984-55-4
1-(8-benzenesulfonyloxy-5-N,N-dimethylaminosulfonylquinolin-2-ylmethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: With sodium carbonate; In acetonitrile; at 60 ℃;
DOI:10.1002/chem.200600379

Reference yield:

: 869984-53-2
8-benzenesulfonyloxy-2-methyl-5-N,N-dimethylaminosulfonylquinoline

: 869984-55-4
1-(8-benzenesulfonyloxy-5-N,N-dimethylaminosulfonylquinolin-2-ylmethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / N-bromosuccinimide; AIBN / CCl₄ / 8 h / Heating

2: 92 percent / Na₂CO₃ / acetonitrile / 60 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium carbonate; In tetrachloromethane; acetonitrile;
DOI:10.1002/chem.200600379

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 869984-55-4
1-(8-benzenesulfonyloxy-5-N,N-dimethylaminosulfonylquinolin-2-ylmethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N / CHCl₃ / 1.5 h / 20 °C

2: 14 percent / N-bromosuccinimide; AIBN / CCl₄ / 8 h / Heating

3: 92 percent / Na₂CO₃ / acetonitrile / 60 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium carbonate; triethylamine; In tetrachloromethane; chloroform; acetonitrile;
DOI:10.1002/chem.200600379