1,3-Dioxolan-4-one, 5-[2-[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methyleth yl]thio]-2,6-bis(1,1-dimethylethyl)phenoxy]ethyl]-2,2-dimethyl-, (5S)-

Base Information

Chemical Name:1,3-Dioxolan-4-one, 5-[2-[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methyleth yl]thio]-2,6-bis(1,1-dimethylethyl)phenoxy]ethyl]-2,2-dimethyl-, (5S)-
CAS No.:870460-32-5
Molecular Formula:C38H58O5S2
Molecular Weight:659.008
Hs Code.:

1,3-Dioxolan-4-one,
5-[2-[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methyleth
yl]thio]-2,6-bis(1,1-dimethylethyl)phenoxy]ethyl]-2,2-dimethyl-, (5S)-

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Chemical Property of 1,3-Dioxolan-4-one, 5-[2-[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methyleth yl]thio]-2,6-bis(1,1-dimethylethyl)phenoxy]ethyl]-2,2-dimethyl-, (5S)-

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Technology Process of 1,3-Dioxolan-4-one, 5-[2-[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methyleth yl]thio]-2,6-bis(1,1-dimethylethyl)phenoxy]ethyl]-2,2-dimethyl-, (5S)-

There total 2 articles about 1,3-Dioxolan-4-one, 5-[2-[4-[[1-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-1-methyleth yl]thio]-2,6-bis(1,1-dimethylethyl)phenoxy]ethyl]-2,2-dimethyl-, (5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23288-49-5
(4,4'-isopropylidenedithio)bis[2,6-di-tert-butylphenol]

: 124724-88-5
(5S)-5-(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-one

: 870460-32-5
2,6-di-tert-butyl-4-(1-{3,5-di-tert-butyl-4-[2-(2,2-dimethyl-[1,3]dioxolan-4(S)-yl)-ethoxy]-phenylsulfanyl}-1-methyl-ethylsulfanyl)-phenol

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 18h;

Reference yield:

: 113278-68-5,114458-03-6,119618-59-6,73991-95-4
2-[(4S)-2,2-dimethyl-5-oxo-1,3-dioxolan-4-yl]acetic acid

: 870460-32-5
2,6-di-tert-butyl-4-(1-{3,5-di-tert-butyl-4-[2-(2,2-dimethyl-[1,3]dioxolan-4(S)-yl)-ethoxy]-phenylsulfanyl}-1-methyl-ethylsulfanyl)-phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 3 h / 0 - 20 °C

1.2: 0 °C

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 18 h / 0 - 20 °C

With borane-THF; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2.1: Mitsunobu reaction;

Reference yield: 79.0%

: 870460-32-5
2,6-di-tert-butyl-4-(1-{3,5-di-tert-butyl-4-[2-(2,2-dimethyl-[1,3]dioxolan-4(S)-yl)-ethoxy]-phenylsulfanyl}-1-methyl-ethylsulfanyl)-phenol

: 870460-33-6
4-{2,6-di-tert-butyl-4-[1-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-1-methyl-ethylsulfanyl]-phen-oxy}-2(S)-hydroxy-butyric aicd

Guidance literature:: 2,6-di-tert-butyl-4-(1-{3,5-di-tert-butyl-4-[2-(2,2-dimethyl-[1,3]dioxolan-4(S)-yl)-ethoxy]-phenylsulfanyl}-1-methyl-ethylsulfanyl)-phenol; With sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water;