2'-Mercaptovalerophenone

Base Information

Chemical Name:2'-Mercaptovalerophenone
CAS No.:870482-30-7
Molecular Formula:C11H14OS
Molecular Weight:194.298
Hs Code.:
DSSTox Substance ID:DTXSID801302142
Nikkaji Number:J2.569.456B

Synonyms:2'-Mercaptovalerophenone;870482-30-7;DTXSID801302142;1-(2-Mercaptophenyl)-1-pentanone

Suppliers and Price of 2'-Mercaptovalerophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2'-Mercaptovalerophenone

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:194.07653624
Heavy Atom Count:13
Complexity:168

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCCC(=O)C1=CC=CC=C1S

Technology Process of 2'-Mercaptovalerophenone

There total 1 articles about 2'-Mercaptovalerophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 109-72-8,29786-93-4
n-butyllithium

: 147-93-3
Thiosalicylic acid

: 870482-30-7
1-(2-sulfanylphenyl)pentan-1-one

Guidance literature:: Thiosalicylic acid; With lithium hydride; In tetrahydrofuran; for 0.5h; Heating;

n-butyllithium; In tetrahydrofuran; diethyl ether; at 20 ℃; for 4h;
DOI:10.1080/10426500590912259

Reference yield: 99.0%

: 870482-30-7
1-(2-sulfanylphenyl)pentan-1-one

: 70-11-1
α-bromoacetophenone

: 1028904-26-8
(3-butylbenzo[b]thiophen-2-yl)(phenyl)methanone

Guidance literature:: 1-(2-sulfanylphenyl)pentan-1-one; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

α-bromoacetophenone; In tetrahydrofuran; at 0 ℃; for 0.5h;

With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Further stages.;
DOI:10.3987/COM-07-11262

Reference yield: 90.0%

: 870482-30-7
1-(2-sulfanylphenyl)pentan-1-one

: 461677-71-4
1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one

: (2S,3R)-1'-benzyl-3-butyl-3-hydroxy-3H-spiro[benzo[b]thiophene-2,3’-indolin]-2’-one

: 1'-benzyl-3-butyl-3-hydroxy-3H-spiro[benzo[b]thiophene-2,3'-indolin]-2'-one

Guidance literature:: With (R)-3,3'-bis(triphenylsilyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; Ru₂(OAc)4; In dichloromethane; at 0 ℃; for 7h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01833