Boronic acid, [2-[[bis(1-methylethyl)amino]carbonyl]phenyl]-, bis(1-methylethyl) ester

Base Information

Chemical Name:Boronic acid, [2-[[bis(1-methylethyl)amino]carbonyl]phenyl]-, bis(1-methylethyl) ester
CAS No.:870530-90-8
Molecular Formula:C19H32BNO3
Molecular Weight:333.279
Hs Code.:

Synonyms:

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Chemical Property of Boronic acid, [2-[[bis(1-methylethyl)amino]carbonyl]phenyl]-, bis(1-methylethyl) ester

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Boronic acid, [2-[[bis(1-methylethyl)amino]carbonyl]phenyl]-, bis(1-methylethyl) ester

There total 1 articles about Boronic acid, [2-[[bis(1-methylethyl)amino]carbonyl]phenyl]-, bis(1-methylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 5419-55-6
Triisopropyl borate

: 20383-28-2
N,N-diisopropyl benzamide

: 870530-90-8
[C₆H₄C(O)N(CH(CH₃)2)2]B(OCH(CH₃)2)2

Guidance literature:: N,N-diisopropyl benzamide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.916667h;

Triisopropyl borate; In tetrahydrofuran; hexane; for 2.25h;
DOI:10.1016/j.jorganchem.2005.07.108

Reference yield: 64.0%

: 870530-90-8
[C₆H₄C(O)N(CH(CH₃)2)2]B(OCH(CH₃)2)2

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 815581-73-8
2-borylated-N,N-diisopropylbenzamide

Guidance literature:: With hydrogenchloride; water; In diethyl ether; for 72h;
DOI:10.1016/j.jorganchem.2005.07.108

Reference yield:

: 870530-90-8
[C₆H₄C(O)N(CH(CH₃)2)2]B(OCH(CH₃)2)2

: 95753-26-7
2-[(N,N-diisopropylamino)methyl]phenylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 64 percent / H₂O; HCl / diethyl ether / 72 h

2.1: sodium borohydride; chlorotrimethylsilane / tetrahydrofuran / 64 h / Heating

2.2: HCl; ammonium chloride / tetrahydrofuran; methanol; H₂O / 20 °C

With hydrogenchloride; sodium tetrahydroborate; chloro-trimethyl-silane; water; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.jorganchem.2005.07.108