2-Hydroxy-3-phenoxypropyl methacrylate

Base Information

• Chemical Name: 2-Hydroxy-3-phenoxypropyl methacrylate
• CAS No.: 16926-87-7
• Deprecated CAS: 162223-14-5
• Molecular Formula: C13H16 O4
• Molecular Weight: 236.268
• Hs Code.: 2916140000
• European Community (EC) Number: 240-994-5
• DSSTox Substance ID: DTXSID40275831,DTXSID80864723
• Nikkaji Number: J195.922K
• Mol file: 16926-87-7.mol

Synonyms:2-hydroxy-3-phenoxypropyl methacrylate;3-phenoxy-2-hydroxypropyl methacrylate;HPPM

Chemical Property of 2-Hydroxy-3-phenoxypropyl methacrylate

Chemical Property:

• Vapor Pressure: 7.58E-07mmHg at 25°C
• Boiling Point: 392°C at 760 mmHg
• PKA: 13.02±0.20(Predicted)
• Flash Point: 147.3°C
• PSA: 55.76000
• Density: 1.131g/cm³
• LogP: 1.54560
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 236.10485899
• Heavy Atom Count: 17
• Complexity: 256

Purity/Quality:

99.9% ^*data from raw suppliers

2-Hydroxy-3-phenoxypropylmethacrylate 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C(=O)OCC(COC1=CC=CC=C1)O

Technology Process of 2-Hydroxy-3-phenoxypropyl methacrylate

There total 6 articles about 2-Hydroxy-3-phenoxypropyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,3-Epoxypropyl methacrylate (106-91-2,25067-05-4,98104-93-9) + sodium phenoxide (139-02-6) → 2-hydroxy-3-phenoxypropyl methacrylate (16926-87-7)

Guidance literature:

sodium phenoxide; With Amberlite IRA-400 resin; In water;

2,3-Epoxypropyl methacrylate; In ethanol; at 50 ℃; for 1.5h;

DOI:10.1081/SCC-200026220

Reference yield: 85.0%

sodium bicarbonate (NaHCO3) + poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + Phenyl glycidyl ether (122-60-1,71031-02-2) → 2-hydroxy-3-phenoxypropyl methacrylate (16926-87-7)

Guidance literature:

With sodium hydroxide; 2,6-di-tert-butyl-4-methyl-phenol; triethylamine; In dichloromethane;

Reference yield: 85.0%

poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + Phenyl glycidyl ether (122-60-1,71031-02-2) → 2-hydroxy-3-phenoxypropyl methacrylate (16926-87-7)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; triethylamine; at 60 ℃; for 24h; Inert atmosphere;

upstream raw materials:

2,3-Epoxypropyl methacrylate

sodium phenoxide

poly(methacrylic acid)

Phenyl glycidyl ether

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