1,5,14-tris(2,3-dihydroxybenzoyl)-10-(1-hydroxy-2-pyridon-6-oyl)-1,5,10,14-tetraazatetradecane

Base Information

Chemical Name:1,5,14-tris(2,3-dihydroxybenzoyl)-10-(1-hydroxy-2-pyridon-6-oyl)-1,5,10,14-tetraazatetradecane
CAS No.:146980-30-5
Molecular Formula:C₃₇H₄₁N₅O₁₂
Molecular Weight:747.759
Hs Code.:
Mol file:146980-30-5.mol

Synonyms:1,5,14-tris(2,3-dihydroxybenzoyl)-10-(1-hydroxy-2-pyridon-6-oyl)-1,5,10,14-tetraazatetradecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,5,14-tris(2,3-dihydroxybenzoyl)-10-(1-hydroxy-2-pyridon-6-oyl)-1,5,10,14-tetraazatetradecane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：269.41000
Density:1.478g/cm³
LogP:3.47380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,5,14-tris(2,3-dihydroxybenzoyl)-10-(1-hydroxy-2-pyridon-6-oyl)-1,5,10,14-tetraazatetradecane

There total 4 articles about 1,5,14-tris(2,3-dihydroxybenzoyl)-10-(1-hydroxy-2-pyridon-6-oyl)-1,5,10,14-tetraazatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026706-00-2
1-Hydroxy-6-oxo-1,6-dihydro-pyridine-2-carboxylic acid [3-(2,3-dimethoxy-benzoylamino)-propyl]-(4-{(2,3-dimethoxy-benzoyl)-[3-(2,3-dimethoxy-benzoylamino)-propyl]-amino}-butyl)-amide

: 146980-30-5
1-Hydroxy-6-oxo-1,6-dihydro-pyridine-2-carboxylic acid [3-(2,3-dihydroxy-benzoylamino)-propyl]-(4-{(2,3-dihydroxy-benzoyl)-[3-(2,3-dihydroxy-benzoylamino)-propyl]-amino}-butyl)-amide

Guidance literature:: With boron tribromide; In dichloromethane; Yield given;
DOI:10.1021/jm00056a011

Reference yield:

: 71-44-3
Spermine

: 146980-30-5
1-Hydroxy-6-oxo-1,6-dihydro-pyridine-2-carboxylic acid [3-(2,3-dihydroxy-benzoylamino)-propyl]-(4-{(2,3-dihydroxy-benzoyl)-[3-(2,3-dihydroxy-benzoylamino)-propyl]-amino}-butyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / CH₂Cl₂ / 3 h

2: 1.) 1,1'-carbonyldiimidazole (CDI)

3: BBr₃ / CH₂Cl₂

With boron tribromide; 1,1'-carbonyldiimidazole; In dichloromethane;
DOI:10.1021/jm00056a011

Reference yield:

: 144344-71-8
3-[(2,3-dimethoxyphenyl)carbonyl]thiazolidine-2-thione

: 146980-30-5
1-Hydroxy-6-oxo-1,6-dihydro-pyridine-2-carboxylic acid [3-(2,3-dihydroxy-benzoylamino)-propyl]-(4-{(2,3-dihydroxy-benzoyl)-[3-(2,3-dihydroxy-benzoylamino)-propyl]-amino}-butyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / CH₂Cl₂ / 3 h

2: 1.) 1,1'-carbonyldiimidazole (CDI)

3: BBr₃ / CH₂Cl₂

With boron tribromide; 1,1'-carbonyldiimidazole; In dichloromethane;
DOI:10.1021/jm00056a011