Boronic acid, [5-octyl-2-(1-pyrrolidinylazo)phenyl]-

Base Information

• Chemical Name: Boronic acid, [5-octyl-2-(1-pyrrolidinylazo)phenyl]-
• CAS No.: 876290-17-4
• Molecular Formula: C₁₈H₃₀BN₃O₂
• Molecular Weight: 331.266
• Mol file: 876290-17-4.mol

Synonyms:

Chemical Property of Boronic acid, [5-octyl-2-(1-pyrrolidinylazo)phenyl]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Boronic acid, [5-octyl-2-(1-pyrrolidinylazo)phenyl]-

There total 1 articles about Boronic acid, [5-octyl-2-(1-pyrrolidinylazo)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H28IN3 (876290-15-2) + Trimethyl borate (121-43-7,63156-11-6) → C18H30BN3O2 (876290-17-4)

Guidance literature:

C₁₈H₂₈IN₃; With n-butyllithium; In diethyl ether; at -78 ℃;

Trimethyl borate; In diethyl ether; at -78 ℃; Further stages.;

DOI:10.1002/chem.200701036

Reference yield:

C18H30BN3O2 (876290-17-4) + para-diiodobenzene (624-38-4,1032416-46-8) → C42H60N6 (876290-20-9)

Guidance literature:

With tri-tert-butyl phosphine; potassium carbonate; dichloro bis(acetonitrile) palladium(II); In 1,4-dioxane; water; at 80 ℃;

DOI:10.1002/chem.200701036

upstream raw materials:

C₁₈H₂₈IN₃

Trimethyl borate

Downstream raw materials:

C₄₂H₆₀N₆