3-Piperidinecarboxylic acid, 6-(acetylamino)-4-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene] amino]-1-(2-ethyl-1-oxobutyl)-5-hydroxy-, diphenylmethyl ester, (3R,4S,5S,6S)-

Base Information

Chemical Name:3-Piperidinecarboxylic acid, 6-(acetylamino)-4-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene] amino]-1-(2-ethyl-1-oxobutyl)-5-hydroxy-, diphenylmethyl ester, (3R,4S,5S,6S)-
CAS No.:876313-91-6
Molecular Formula:C38H53N5O9
Molecular Weight:723.867
Hs Code.:

3-Piperidinecarboxylic acid,
6-(acetylamino)-4-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]
amino]-1-(2-ethyl-1-oxobutyl)-5-hydroxy-, diphenylmethyl ester,
(3R,4S,5S,6S)-

Synonyms:

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Chemical Property of 3-Piperidinecarboxylic acid, 6-(acetylamino)-4-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene] amino]-1-(2-ethyl-1-oxobutyl)-5-hydroxy-, diphenylmethyl ester, (3R,4S,5S,6S)-

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Technology Process of 3-Piperidinecarboxylic acid, 6-(acetylamino)-4-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene] amino]-1-(2-ethyl-1-oxobutyl)-5-hydroxy-, diphenylmethyl ester, (3R,4S,5S,6S)-

There total 4 articles about 3-Piperidinecarboxylic acid, 6-(acetylamino)-4-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene] amino]-1-(2-ethyl-1-oxobutyl)-5-hydroxy-, diphenylmethyl ester, (3R,4S,5S,6S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 876313-90-5
(3R,4S,5S,6S)-6-Acetylamino-4-amino-1-(2-ethyl-butyryl)-5-hydroxy-piperidine-3-carboxylic acid benzhydryl ester

: 145013-05-4
tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

: 876313-91-6
C₃₈H₅₃N₅O₉

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2005.10.055

Reference yield:

: 876313-88-1
(3aS,4S,7R,7aS)-4-Acetylamino-5-(2-ethyl-butyryl)-2-trichloromethyl-3a,4,5,6,7,7a-hexahydro-oxazolo[5,4-c]pyridine-7-carboxylic acid benzhydryl ester

: 876313-91-6
C₃₈H₅₃N₅O₉

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / aq. p-toluenesulfonic acid; pyridine / 2 h / 80 °C

2: 57 percent / sodium borohydride / ethanol / 2 h / 20 °C

3: 95 percent / mercuric chloride; Et₃N / dimethylformamide / 2 h / 20 °C

With pyridine; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; mercury dichloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.10.055

Reference yield:

: 876313-89-2
(3R,4S,5S,6S)-6-Acetylamino-1-(2-ethyl-butyryl)-5-hydroxy-4-(2,2,2-trichloro-acetylamino)-piperidine-3-carboxylic acid benzhydryl ester

: 876313-91-6
C₃₈H₅₃N₅O₉

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / sodium borohydride / ethanol / 2 h / 20 °C

2: 95 percent / mercuric chloride; Et₃N / dimethylformamide / 2 h / 20 °C

With sodium tetrahydroborate; triethylamine; mercury dichloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2005.10.055