4-methyl-6-{[(2-{[(Z)-(3-methyl-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]amino}ethyl)amino]methylidene}cyclohexa-2,4-dien-1-one

Base Information

Chemical Name:4-methyl-6-{[(2-{[(Z)-(3-methyl-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]amino}ethyl)amino]methylidene}cyclohexa-2,4-dien-1-one
CAS No.:6943-13-1
Molecular Formula:C18H20 N2 O2
Molecular Weight:296.369
Hs Code.:

Synonyms:2,4-Xylenol,a2,a2'-(ethylenedinitrilo)di- (7CI);N,N'-Ethylenebis(5-methylsalicylideneamine); NSC 51651

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-6-{[(2-{[(Z)-(3-methyl-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]amino}ethyl)amino]methylidene}cyclohexa-2,4-dien-1-one

Chemical Property:

Vapor Pressure:2.81E-10mmHg at 25°C
Boiling Point:503.8°Cat760mmHg
Flash Point:181°C
PSA：65.18000
Density:1.242g/cm³
LogP:3.25260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-methyl-6-{[(2-{[(Z)-(3-methyl-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]amino}ethyl)amino]methylidene}cyclohexa-2,4-dien-1-one

There total 2 articles about 4-methyl-6-{[(2-{[(Z)-(3-methyl-6-oxocyclohexa-2,4-dien-1-ylidene)methyl]amino}ethyl)amino]methylidene}cyclohexa-2,4-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 613-84-3
2-hydroxy-5-methylbenzaldehyde

: 107-15-3,85404-18-8
ethylenediamine

: 6943-13-1
bis-(5-methyl-salicylidene)-ethylenediamine

Guidance literature:: In methanol; at 20 ℃; for 0.5h;
DOI:10.1134/S1070328417050062

Reference yield:

: 106-44-5
p-cresol

: 6943-13-1
bis-(5-methyl-salicylidene)-ethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: glycerol; boric acid / 150 - 160 °C / in einem zuvor auf 165grad erhitzten Gemisch von Glycerin und Borsaeure auf 150-160grad und Behandeln des auf 110grad abgekuehlten Reaktionsgemisches mit wss. H₂SO₄ unter Durchleiten von Wasserdampf

2: ethanol; water / 60 °C

With ethanol; water; boric acid; glycerol;