Technology Process of 2-Butanol, 3-azido-1,4-bis(phenylmethoxy)-, (2R,3R)-
There total 6 articles about 2-Butanol, 3-azido-1,4-bis(phenylmethoxy)-, (2R,3R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
porcine liver esterase;
In
aq. phosphate buffer;
at 35 ℃;
for 168h;
pH=7.4;
Green chemistry;
Enzymatic reaction;
DOI:10.1016/j.tetlet.2020.152717
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 0 - 20 °C
2: sodium azide / N,N-dimethyl-formamide / 24 h / 100 °C / Inert atmosphere
3: pyridine / 1.5 h / 20 °C
4: porcine liver esterase / aq. phosphate buffer / 168 h / 35 °C / pH 7.4 / Green chemistry; Enzymatic reaction
With
pyridine; porcine liver esterase; sodium azide; 3-chloro-benzenecarboperoxoic acid;
In
aq. phosphate buffer; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2020.152717
