tert-butyl 2-oxopropane-1,3-diyldicarbamate

Base Information

• Chemical Name: tert-butyl 2-oxopropane-1,3-diyldicarbamate
• CAS No.: 877317-26-5
• Molecular Formula: C16H22N2O5
• Molecular Weight: 322.361
• Mol file: 877317-26-5.mol

Synonyms:

Chemical Property of tert-butyl 2-oxopropane-1,3-diyldicarbamate

Chemical Property:

• PSA: 93.73000
• LogP: 2.78840

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl 2-oxopropane-1,3-diyldicarbamate

There total 1 articles about tert-butyl 2-oxopropane-1,3-diyldicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

benzyl tert-butyl (2-hydroxypropane-1,3-diyl)dicarbamate (877317-25-4) → C16H22N2O5 (877317-26-5)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 - 25 ℃;

Reference yield: 64.0%

C16H22N2O5 (877317-26-5) → C18H24N4O6 (877317-27-6)

Guidance literature:

With ammonium carbonate; potassium cyanide; In ethanol; water; at 80 ℃;

Reference yield: 56.0%

C16H22N2O5 (877317-26-5) + methylmagnesium bromide (75-16-1) → C17H26N2O5

Guidance literature:

In tetrahydrofuran; at -65 - 20 ℃; for 2.5h; Inert atmosphere;

upstream raw materials:

benzyl tert-butyl (2-hydroxypropane-1,3-diyl)dicarbamate

Downstream raw materials:

C₁₈H₂₄N₄O₆

Refernces