Cyclohexene, 6-(2-bromoethyl)-1,6-dimethyl-4-(1-methylethenyl)-, (4R,6S)-

Base Information

Chemical Name:Cyclohexene, 6-(2-bromoethyl)-1,6-dimethyl-4-(1-methylethenyl)-, (4R,6S)-
CAS No.:877856-32-1
Molecular Formula:C13H21Br
Molecular Weight:257.214
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexene, 6-(2-bromoethyl)-1,6-dimethyl-4-(1-methylethenyl)-, (4R,6S)-

Chemical Property:

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Technology Process of Cyclohexene, 6-(2-bromoethyl)-1,6-dimethyl-4-(1-methylethenyl)-, (4R,6S)-

There total 5 articles about Cyclohexene, 6-(2-bromoethyl)-1,6-dimethyl-4-(1-methylethenyl)-, (4R,6S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 328934-89-0
(-)-(3R,5R)-3-(2-hydroxyethyl)-5-isopropenyl-2,3-dimethylcyclohexane

: 877856-32-1
(3R,5R)-(2-bromoethyl)-5-isopropenyl-2,3-dimethylcyclohexene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 6485-40-1,2244-16-8
(R)-Carvone

: 877856-32-1
(3R,5R)-(2-bromoethyl)-5-isopropenyl-2,3-dimethylcyclohexene

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / pyridinium chlorochromate; silica gel / diethyl ether; CH₂Cl₂

2: 95 percent / LiAlH₄ / diethyl ether / -70 °C

3: 80 percent / propionic acid / 120 h / 160 °C

4: 90 percent / LiAlH₄ / diethyl ether / 2 h / 20 °C

5: 100 percent / CBr₄; P(C₆H₅)3 / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; silica gel; propionic acid; triphenylphosphine; pyridinium chlorochromate; In diethyl ether; dichloromethane;

Reference yield:

: 85710-65-2,85710-66-3
(5S)-2,3-Dimethyl-5-isopropenylcyclohex-2-en-1-one

: 877856-32-1
(3R,5R)-(2-bromoethyl)-5-isopropenyl-2,3-dimethylcyclohexene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / LiAlH₄ / diethyl ether / -70 °C

2: 80 percent / propionic acid / 120 h / 160 °C

3: 90 percent / LiAlH₄ / diethyl ether / 2 h / 20 °C

4: 100 percent / CBr₄; P(C₆H₅)3 / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; carbon tetrabromide; propionic acid; triphenylphosphine; In diethyl ether; dichloromethane;