ethyl (2E)-2-cyano-2-[4-(2-ethoxy-2-oxoethyl)-1,3-dithiol-2-ylidene]acetate

Base Information

Chemical Name:ethyl (2E)-2-cyano-2-[4-(2-ethoxy-2-oxoethyl)-1,3-dithiol-2-ylidene]acetate
CAS No.:88406-73-9
Molecular Formula:C₁₂H₁₃NO₄S₂
Molecular Weight:299.372
Hs Code.:
NSC Number:373932
DSSTox Substance ID:DTXSID20419615
Wikidata:Q82230716

Synonyms:NSC373932;88406-73-9;DTXSID20419615;NSC-373932

Suppliers and Price of ethyl (2E)-2-cyano-2-[4-(2-ethoxy-2-oxoethyl)-1,3-dithiol-2-ylidene]acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of ethyl (2E)-2-cyano-2-[4-(2-ethoxy-2-oxoethyl)-1,3-dithiol-2-ylidene]acetate

Chemical Property:

Vapor Pressure:3.16E-06mmHg at 25°C
Boiling Point:388°Cat760mmHg
Flash Point:188.5°C
Density:1.331g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:299.02860024
Heavy Atom Count:19
Complexity:487

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC1=CSC(=C(C#N)C(=O)OCC)S1
Isomeric SMILES:CCOC(=O)CC1=CS/C(=C(/C#N)\C(=O)OCC)/S1

Technology Process of ethyl (2E)-2-cyano-2-[4-(2-ethoxy-2-oxoethyl)-1,3-dithiol-2-ylidene]acetate

There total 3 articles about ethyl (2E)-2-cyano-2-[4-(2-ethoxy-2-oxoethyl)-1,3-dithiol-2-ylidene]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 88406-71-7
ethyl 2-cyano(ethoxycarbonyl)methylene-4-hydroxy-1,3-dithiolane-4-acetate

: 88406-73-9
ethyl 2-cyano(ethoxycarbonyl)methylene-1,3-dithiole-4-acetate

Guidance literature:: With acetic anhydride; at 110 ℃; for 96h;

Reference yield:

: 13176-46-0
4-bromoethyl acetoacetate

: 88406-73-9
ethyl 2-cyano(ethoxycarbonyl)methylene-1,3-dithiole-4-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 60percent sodium hydride / tetrahydrofuran / 1 h / 0 °C

2: 60 percent / acetic anhydride / 96 h / 110 °C

With acetic anhydride; sodium hydride; In tetrahydrofuran;

Reference yield:

: 105-56-6
ethyl 2-cyanoacetate

: 88406-73-9
ethyl 2-cyano(ethoxycarbonyl)methylene-1,3-dithiole-4-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 60percent sodium hydride / tetrahydrofuran / 1 h / 0 °C

2: 60 percent / acetic anhydride / 96 h / 110 °C

With acetic anhydride; sodium hydride; In tetrahydrofuran;