Technology Process of Benzoic acid, 2-(chloromethyl)-4,6-dimethoxy-3-methyl-
There total 9 articles about Benzoic acid, 2-(chloromethyl)-4,6-dimethoxy-3-methyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogen phosphate;
In
dimethyl sulfoxide;
at 20 ℃;
DOI:10.1002/jhet.5570430105
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 79 percent / carbon tetrachloride; triphenyl phosphine
2: 95 percent / methanol
3: 93 percent / phosphoryl chloride / 70 - 80 °C
4: 89 percent / aq. NH2NH2; KOH
5: 75 percent / phosphoryl chloride / 8 h / 80 - 90 °C
6: 61 percent / aq. sodium dihydrogen phosphate; sodium chlorite / dimethylsulfoxide / 20 °C
With
tetrachloromethane; potassium hydroxide; sodium chlorite; sodium dihydrogen phosphate; hydrazine hydrate; triphenylphosphine; trichlorophosphate;
In
methanol; dimethyl sulfoxide;
3: Vilsmeier formylation / 4: Wolf-Kishner reduction / 5: Vilsmeier formylation;
DOI:10.1002/jhet.5570430105
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / methanol
2: 93 percent / phosphoryl chloride / 70 - 80 °C
3: 89 percent / aq. NH2NH2; KOH
4: 75 percent / phosphoryl chloride / 8 h / 80 - 90 °C
5: 61 percent / aq. sodium dihydrogen phosphate; sodium chlorite / dimethylsulfoxide / 20 °C
With
potassium hydroxide; sodium chlorite; sodium dihydrogen phosphate; hydrazine hydrate; trichlorophosphate;
In
methanol; dimethyl sulfoxide;
2: Vilsmeier formylation / 3: Wolf-Kishner reduction / 4: Vilsmeier formylation;
DOI:10.1002/jhet.5570430105
