1H-Pyrrole-2-carboxylic acid, 5-[[[[[(1,1-dimethylethoxy)carbonyl]amino][(6-methoxy-6-oxohexyl)amino ]methylene]amino]carbonyl]-, phenylmethyl ester

Base Information

Chemical Name:1H-Pyrrole-2-carboxylic acid, 5-[[[[[(1,1-dimethylethoxy)carbonyl]amino][(6-methoxy-6-oxohexyl)amino ]methylene]amino]carbonyl]-, phenylmethyl ester
CAS No.:878627-31-7
Molecular Formula:C26H34N4O7
Molecular Weight:514.579
Hs Code.:

1H-Pyrrole-2-carboxylic acid,
5-[[[[[(1,1-dimethylethoxy)carbonyl]amino][(6-methoxy-6-oxohexyl)amino
]methylene]amino]carbonyl]-, phenylmethyl ester

Synonyms:

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Chemical Property of 1H-Pyrrole-2-carboxylic acid, 5-[[[[[(1,1-dimethylethoxy)carbonyl]amino][(6-methoxy-6-oxohexyl)amino ]methylene]amino]carbonyl]-, phenylmethyl ester

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Technology Process of 1H-Pyrrole-2-carboxylic acid, 5-[[[[[(1,1-dimethylethoxy)carbonyl]amino][(6-methoxy-6-oxohexyl)amino ]methylene]amino]carbonyl]-, phenylmethyl ester

There total 2 articles about 1H-Pyrrole-2-carboxylic acid, 5-[[[[[(1,1-dimethylethoxy)carbonyl]amino][(6-methoxy-6-oxohexyl)amino ]methylene]amino]carbonyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-[(tert-butoxycarbonylamino-trifluoromethanesulfonylimino-methyl)-carbamoyl]-1H-pyrrole-2-carboxylic acid benzyl ester

: 1926-80-3
methyl 6-aminocaproate hydrochloride

: 878627-31-7
C₂₆H₃₄N₄O₇

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ja056465c

Reference yield:

: 878627-28-2
5-((tert-butyloxycarbonyl)guanidiniocarbonyl)-1H-pyrrole-2-carboxylic acid benzyl ester

: 878627-31-7
C₂₆H₃₄N₄O₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / CH₂Cl₂ / 1 h / 0 °C

1.2: CH₂Cl₂ / 29 h / -60 - 20 °C

2.1: 3.4 g / Et₃N / CH₂Cl₂ / 24 h / 20 °C

With sodium hydride; triethylamine; In dichloromethane;
DOI:10.1021/ja056465c