Carbamic acid, [(1R)-3-[[(2S)-2-[(benzo[b]thien-2-ylcarbonyl)amino]-4-methyl-1-oxopent yl]amino]-1-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]propyl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [(1R)-3-[[(2S)-2-[(benzo[b]thien-2-ylcarbonyl)amino]-4-methyl-1-oxopent yl]amino]-1-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]propyl]-, phenylmethyl ester
CAS No.:878799-30-5
Molecular Formula:C35H36N4O6S
Molecular Weight:640.76
Hs Code.:

Carbamic acid,
[(1R)-3-[[(2S)-2-[(benzo[b]thien-2-ylcarbonyl)amino]-4-methyl-1-oxopent
yl]amino]-1-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]propyl]-,
phenylmethyl ester

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Chemical Property of Carbamic acid, [(1R)-3-[[(2S)-2-[(benzo[b]thien-2-ylcarbonyl)amino]-4-methyl-1-oxopent yl]amino]-1-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]propyl]-, phenylmethyl ester

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Technology Process of Carbamic acid, [(1R)-3-[[(2S)-2-[(benzo[b]thien-2-ylcarbonyl)amino]-4-methyl-1-oxopent yl]amino]-1-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]propyl]-, phenylmethyl ester

There total 1 articles about Carbamic acid, [(1R)-3-[[(2S)-2-[(benzo[b]thien-2-ylcarbonyl)amino]-4-methyl-1-oxopent yl]amino]-1-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]propyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 215941-14-3
(benzo[b]thiophene-2-carbonyl)-l-leucine

: 878799-29-2
phenylmethyl (2R)-4-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]butanoate

: 878799-30-5
phenylmethyl {(1R)-3-{[N-(1-benzothien-2-ylcarbonyl)-L-leucyl]amino}-1-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]propyl}carbamate

Guidance literature:: phenylmethyl (2R)-4-({[(1,1-dimethylethyl)oxy]carbonyl}amino)-2-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]butanoate; With hydrogenchloride; In 1,4-dioxane; methanol; dichloromethane; at 20 ℃; for 2h;

(benzo[b]thiophene-2-carbonyl)-l-leucine; With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In dichloromethane; at 20 ℃;

Reference yield: 40.0%

: 878799-30-5
phenylmethyl {(1R)-3-{[N-(1-benzothien-2-ylcarbonyl)-L-leucyl]amino}-1-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]propyl}carbamate

: 85958-57-2
2-chloro-4-fluorobenzene-1-sulfonyl chloride

: 878799-31-6
N-[(1S)-1-({[(3R)-3-{[(2-chloro-4-fluorophenyl)sulfonyl]amino}-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)butyl]amino}carbonyl)-3-methylbutyl]-1-benzothiophene-2-carboxamide

Guidance literature:: phenylmethyl {(1R)-3-{[N-(1-benzothien-2-ylcarbonyl)-L-leucyl]amino}-1-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]propyl}carbamate; With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 2h;

2-chloro-4-fluorobenzene-1-sulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 3h;