Stannane, docosyltriphenyl-

Base Information

Chemical Name:Stannane, docosyltriphenyl-
CAS No.:879279-32-0
Molecular Formula:C₄₀H₆₀Sn
Molecular Weight:659.626
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, docosyltriphenyl-

Chemical Property:

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Technology Process of Stannane, docosyltriphenyl-

There total 1 articles about Stannane, docosyltriphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 6938-66-5
1-Bromodocosane

: 639-58-7
triphenyltin chloride

: 879279-32-0
triphenyldocosyltin

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: MgBrCl; (N2); using Schlenk techniques; reflux of mixt. of BrC22H45 and Mg in THF; addn. via canula to soln. of SnPh3Cl in THF cooled at 0°C; warming to room temp., reflux for 1 h; treatment with satd. soln. of NH4Cl; extn. into petroleum ether; washingwith H2O; drying over MgSO4; chromy. over silica gel (elution gradient petroleum ether/ethyl acetate from 100:0 to 97:3 (v/v)); elem. anal.;
DOI:10.1021/om700534j

Reference yield: 99.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 879279-32-0
triphenyldocosyltin

: docosylphenyltin dichloride

Guidance literature:: In diethyl ether; (N2); using Schlenk techniques; treatment of docosyltriphenyltin with slight excess (4 equiv.) of anhyd. HCl in Et2O for 48 h;
DOI:10.1021/om700534j