methyl 4-(benzyloxy)-5,7-dimethoxynaphthalene-2-carboxylate

Base Information

Chemical Name:methyl 4-(benzyloxy)-5,7-dimethoxynaphthalene-2-carboxylate
CAS No.:879885-56-0
Molecular Formula:C21H20O5
Molecular Weight:352.38100
Hs Code.:

Synonyms:methyl 4-benzyloxy-3-nitrophenylacetate;methyl 4-benzyloxy-5,7-dimethoxy-2-naphthoate;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(benzyloxy)-5,7-dimethoxynaphthalene-2-carboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:521.096oC at 760 mmHg
Flash Point:228.725oC
PSA：53.99000
Density:1.198g/cm3
LogP:4.22260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 4-(benzyloxy)-5,7-dimethoxynaphthalene-2-carboxylate

There total 1 articles about methyl 4-(benzyloxy)-5,7-dimethoxynaphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 78395-68-3
methyl 4-hydroxy-5,7-dimethoxy-2-naphthoate

: 100-39-0
benzyl bromide

: 879885-56-0
methyl 4-benzyloxy-5,7-dimethoxy-2-naphthoate

: methyl 2-benzyl-4-hydroxy-5,7-dimethoxy-2-naphthoate

Guidance literature:: With potassium carbonate; In acetone; for 18h; Heating;
DOI:10.1080/00397910500377370

Reference yield: 85.0%

: 879885-56-0
methyl 4-benzyloxy-5,7-dimethoxy-2-naphthoate

: 879885-58-2
4-benzyloxy-2-hydroxymethyl-5,7-dimethoxynaphthalene

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 23 ℃;
DOI:10.1080/00397910500377370

Reference yield:

: 879885-56-0
methyl 4-benzyloxy-5,7-dimethoxy-2-naphthoate

: 879885-59-3
2-acetoxymethyl-4-benzyloxy-5,7-dimethoxynaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / lithium aluminium hydride / tetrahydrofuran / 23 °C

2: 97 percent / pyridine / 24 h / 23 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1080/00397910500377370