Technology Process of Phenol, 3,5-dimethoxy-4-[(methylamino)methyl]-
There total 3 articles about Phenol, 3,5-dimethoxy-4-[(methylamino)methyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium dihydroxide;
In
methanol; ethyl acetate;
at 20 ℃;
for 20h;
DOI:10.1021/ol052891r
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / potassium carbonate / dimethylformamide / 21 h
2: 66 percent / sodium cyanoborohydride / methanol / 48 h / 20 °C
3: 85 percent / hydrogen / Pd(OH)2/C / ethyl acetate; methanol / 20 h / 20 °C
With
hydrogen; sodium cyanoborohydride; potassium carbonate;
palladium dihydroxide;
In
methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ol052891r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 66 percent / sodium cyanoborohydride / methanol / 48 h / 20 °C
2: 85 percent / hydrogen / Pd(OH)2/C / ethyl acetate; methanol / 20 h / 20 °C
With
hydrogen; sodium cyanoborohydride;
palladium dihydroxide;
In
methanol; ethyl acetate;
DOI:10.1021/ol052891r
